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Mechanochemical Synthesis of Chemically Stable Isoreticular Covalent Organic Frameworks
Abstract
Three thermally and chemically stable isoreticular covalent organic frameworks (COFs) were synthesized via room-temperature solvent-free mechanochemical grinding. These COFs were successfully compared with their solvothermally synthesized counterparts in all aspects. These solvent-free mechanochemically synthesized COFs have moderate crystallinity with remarkable stability in boiling water, acid (9 N HCl), and base [TpBD (MC) in 3 N NaOH and TpPa-2 (MC) in 9 N NaOH]. Exfoliation of COF layers was simultaneously observed with COF formation during mechanochemical synthesis. The structures thus obtained seemed to have a graphene-like layered morphology (exfoliated layers), unlike the parent COFs synthesized solvothermally.
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Cited by
Stable, crystalline, porous, covalent organic frameworks as a platform for chiral organocatalysts
Xu, H., Gao, J., & Jiang, D. (2015) · Nature Chemistry · doi:10.1038/nchem.2352 · Cited by 1,643
Covalent Organic Framework Photocatalysts: Structures and Applications
Wang, H., Wang, H., Wang, Z., Tang, L., Zeng, G., Xu, P., Chen, M., Xiong, T., Zhou, C., Li, X., et al. (2020) · Chemical Society Reviews · doi:10.1039/d0cs00278j · Cited by 1,301
Wang, H., Zeng, Z., Xu, P., Li, L., Zeng, G., Xiao, R., Tang, Z., Huang, D., Tang, L., Lai, C., et al. (2019) · Chemical Society Reviews · doi:10.1039/c8cs00376a · Cited by 804
Interface-Assisted Synthesis of 2D Materials: Trend and Challenges
Dong, R., Zhang, T., & Feng, X. (2018) · Chemical Reviews · doi:10.1021/acs.chemrev.8b00056 · Cited by 710
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Meng, X., & Xiao, F.-S. (2014) · Chemical Reviews · doi:10.1021/cr4001513 · Cited by 635
Metadata
- Authors
- Biswal, B. P., Chandra, S., Kandambeth, S., Lukose, B., Heine, T., & Banerjee, R.
- Venue
- Journal of the American Chemical Society
- Publisher
- American Chemical Society (ACS)
- Published
- 2013-03-29
- Volume
- 135
- Issue
- 14
- Pages
- 5328-5331
- ISSN
- 0002-7863 (ISSN-L)
- 1520-5126
- OpenAlex
- W2059935405
- Cited by
- 1,240
- References
- 0
- FWCI
- 15.10
- Type
- journal article
- Language
- en
- Open access
- closed
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- Biswal, B. P., Chandra, S., Kandambeth, S., Lukose, B., Heine, T., & Banerjee, R. (2013). Mechanochemical Synthesis of Chemically Stable Isoreticular Covalent Organic Frameworks. Journal of the American Chemical Society. https://doi.org/10.1021/ja4017842
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