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Nonaqueous Production of Nanostructured Anatase with High-Energy Facets
Abstract
Although solution-based synthesis is the most powerful and economic method to create nanostructured anatase TiO(2), under those synthesis conditions the {101} facets are the most thermodynamically stable, making it difficult to create anatase nanomaterials with a large percentage of high-energy {001} or {010} facets exposed. Here, we report a facile nonaqueous synthetic route to prepare anatase nanosheets with exposed {001} facets and high-quality rhombic-shaped anatase nanocrystals with a large percentage of exposed {010} facets. Including adscititious water in the nonaqueous synthesis and eliminating the use of carboxylic acid type capping agents are the two keys to integrating the structural diversity from aqueous systems into large-quantity synthesis in nonaqueous systems. The nanostructured TiO(2) that we prepared exhibits conspicuous activity in the photocatalytic degradation of organic contaminants.
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Cited by
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Chen, X., Shen, S., Guo, L., & Mao, S. S. (2010) · Chemical Reviews · doi:10.1021/cr1001645 · Cited by 7,876
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Luttrell, T., Halpegamage, S., Tao, J., Kramer, A., Sutter, E., & Batzill, M. (2014) · Scientific Reports · doi:10.1038/srep04043 · Cited by 1,544
Facet Effect of Single-Crystalline Ag3PO4 Sub-microcrystals on Photocatalytic Properties
Bi, Y., Ouyang, S., Umezawa, N., Cao, J., & Ye, J. (2011) · Journal of the American Chemical Society · doi:10.1021/ja2002132 · Cited by 1,316
Titanium Dioxide Crystals with Tailored Facets
Liu, G., Yang, H. G., Pan, J., Yang, Y. Q., Lu, G. Q. (., & Cheng, H.-M. (2014) · Chemical Reviews · doi:10.1021/cr400621z · Cited by 1,084
Nanostructured metal oxide-based materials as advanced anodes for lithium-ion batteries
Wu, H. B., Chen, J. S., Hng, H. H., & Wen (David) Lou, X. (2012) · Nanoscale · doi:10.1039/c2nr11966h · Cited by 1,082
Metadata
- Authors
- Wu, B., Guo, C., Zheng, N., Xie, Z., & Stucky, G. D.
- Venue
- Journal of the American Chemical Society
- Publisher
- American Chemical Society (ACS)
- Published
- 2008-12-24
- Volume
- 130
- Issue
- 51
- Pages
- 17563-17567
- ISSN
- 0002-7863 (ISSN-L)
- 1520-5126
- OpenAlex
- W1982578528
- Cited by
- 406
- References
- 0
- FWCI
- 18.11
- Type
- journal article
- Language
- en
- Open access
- closed
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- Wu, B., Guo, C., Zheng, N., Xie, Z., & Stucky, G. D. (2008). Nonaqueous Production of Nanostructured Anatase with High-Energy Facets. Journal of the American Chemical Society. https://doi.org/10.1021/ja8069715
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