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Consolidation of Metal Oxide Nanocrystals. Reactive Pellets with Controllable Pore Structure That Represent a New Family of Porous, Inorganic Materials
Abstract
Nanocrystals of MgO (4 nm) exist as polyhedral structures with high surface concentrations of edge/corner sites. In powder form the crystallites weakly agglomerate into porous weblike structures of approximately 1400 nm according to small-angle X-ray scattering. Upon consolidation of these fine powders under pressure, pellets can be readily prepared that maintain their high surface areas, and small crystallite sizes. In addition, large pore volumes and pore size openings can be controllably decreased with pelletization pressure increase. The pellets retain their voracious adsorbent affinities and capacities for a wide variety of organic molecules and acid gases. Quantitative measurements on the adsorption of a series of alcohols vs pelletization pressure reveal a pattern of molecular size selectivity.
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Cited by
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Stoimenov, P. K., Klinger, R. L., Marchin, G. L., & Klabunde, K. J. (2002) · Langmuir · doi:10.1021/la0202374 · Cited by 1,887
Self-citationKhezerlou, A., Alizadeh-Sani, M., Azizi-Lalabadi, M., & Ehsani, A. (2018) · Microbial Pathogenesis · doi:10.1016/j.micpath.2018.08.008 · Cited by 404
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Rolison, D. R., & Dunn, B. (2001) · Journal of Materials Chemistry · doi:10.1039/b007591o · Cited by 357
Li, Y., Peng, Y.-K., Hu, L., Zheng, J., Prabhakaran, D., Wu, S., Puchtler, T. J., Li, M., Wong, K.-Y., Taylor, R. A., et al. (2019) · Nature Communications · doi:10.1038/s41467-019-12385-1 · Cited by 267
Metadata
- Authors
- Richards, R., Li, W., Decker, S., Davidson, C., Koper, O., Zaikovski, V., Volodin, A., Rieker, T., & Klabunde, K. J.
- Venue
- Journal of the American Chemical Society
- Publisher
- American Chemical Society (ACS)
- Published
- 2000-05-01
- Volume
- 122
- Issue
- 20
- Pages
- 4921-4925
- ISSN
- 0002-7863 (ISSN-L)
- 1520-5126
- OpenAlex
- W1986015613
- Cited by
- 249
- References
- 0
- FWCI
- 6.80
- Type
- journal article
- Language
- en
- Open access
- closed
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- Richards, R., Li, W., Decker, S., Davidson, C., Koper, O., Zaikovski, V., Volodin, A., Rieker, T., & Klabunde, K. J. (2000). Consolidation of Metal Oxide Nanocrystals. Reactive Pellets with Controllable Pore Structure That Represent a New Family of Porous, Inorganic Materials. Journal of the American Chemical Society. https://doi.org/10.1021/ja994383g
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Contains information from the Semantic Scholar Academic Graph Datasets, made available under the ODC Attribution License (ODC-BY 1.0).
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