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Perovskite CH3NH3PbI3(Cl) Single Crystals: Rapid Solution Growth, Unparalleled Crystalline Quality, and Low Trap Density toward 108 cm–3
Abstract
Single crystal reflects the intrinsic physical properties of a material, and single crystals with high-crystalline quality are highly desired for the acquisition of high-performance devices. We found that large single crystals of perovskite CH3NH3PbI3(Cl) could be grown rapidly from chlorine-containing solutions. Within 5 days, CH3NH3PbI3(Cl) single crystal as large as 20 mm × 18 mm × 6 mm was harvested. As a most important index to evaluate the crystalline quality, the full width at half-maximum (fwhm) in the high-resolution X-ray rocking curve (HR-XRC) of as-grown CH3NH3PbI3(Cl) single crystal was measured as 20 arcsec, which is far superior to so far reported CH3NH3PbI3 single crystals (∼1338 arcsec). The unparalleled crystalline quality delivered a low trap-state density of down to 7.6 × 10(8) cm(-3), high carrier mobility of 167 ± 35 cm(2) V(-1) s(-1), and long transient photovoltaic carrier lifetime of 449 ± 76 μs. The improvement in the crystalline quality, together with the rapid growth rate and excellent carrier transport property, provides state-of-the-art single crystalline hybrid perovskite materials for high-performance optoelectronic devices.
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Stranks, S. D., Eperon, G. E., Grancini, G., Menelaou, C., Alcocer, M. J. P., Leijtens, T., Herz, L. M., Petrozza, A., & Snaith, H. J. (2013) · Science · doi:10.1126/science.1243982 · Cited by 10,413
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Han, C., Wang, J., Zhang, S., Chen, L., Bi, F., Wang, J., Yang, C., Wang, P., Li, Y., & Bao, X. (2023) · Advanced Materials · doi:10.1002/adma.202208986 · Cited by 308
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Metadata
- Authors
- Lian, Z., Yan, Q., Gao, T., Ding, J., Lv, Q., Ning, C., Li, Q., & Sun, J.-L.
- Venue
- Journal of the American Chemical Society
- Publisher
- American Chemical Society (ACS)
- Published
- 2016-07-26
- Volume
- 138
- Issue
- 30
- Pages
- 9409-9412
- ISSN
- 0002-7863 (ISSN-L)
- 1520-5126
- OpenAlex
- W2486439229
- Cited by
- 297
- References
- 1
- FWCI
- 12.81
- Type
- journal article
- Language
- en
- Open access
- closed
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- Lian, Z., Yan, Q., Gao, T., Ding, J., Lv, Q., Ning, C., Li, Q., & Sun, J.-L. (2016). Perovskite CH3NH3PbI3(Cl) Single Crystals: Rapid Solution Growth, Unparalleled Crystalline Quality, and Low Trap Density toward 108 cm–3. Journal of the American Chemical Society. https://doi.org/10.1021/jacs.6b05683
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