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A Study of the Ionic Liquid Mediated Microwave Heating of Organic Solvents
Abstract
The use of ionic liquids as aids for microwave heating of nonpolar solvents has been investigated. We show that hexane and toluene together with solvents such as THF and dioxane can be heated way above their boiling point in sealed vessels using a small quantity of an ionic liquid, thereby allowing them to be used as media for microwave-assisted chemistry. Using the appropriate ionic liquid, the heating can be performed with no contamination of the solvent. To show the applicability of the system, two test reactions have been successfully performed.
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Cites
Preparation and polymerization of new organic molten salts; N-alkylimidazolium salt derivatives
Hirao, M., Ito, K., & Ohno, H. (2000) · Electrochimica Acta · doi:10.1016/s0013-4686(99)00334-5 · Cited by 179
Cited by
Gawande, M. B., Shelke, S. N., Zboril, R., & Varma, R. S. (2014) · Accounts of Chemical Research · doi:10.1021/ar400309b · Cited by 774
Singh, T., & Kumar, A. (2007) · The Journal of Physical Chemistry B · doi:10.1021/jp0726889 · Cited by 455
Chianese, A. R., Kovacevic, A., Zeglis, B. M., Faller, J. W., & Crabtree, R. H. (2004) · Organometallics · doi:10.1021/om049903h · Cited by 329
Zeolite Synthesis under Nonconventional Conditions: Reagents, Reactors, and Modi Operandi
Deneyer, A., Ke, Q., Devos, J., & Dusselier, M. (2020) · Chemistry of Materials · doi:10.1021/acs.chemmater.9b04741 · Cited by 82
Metadata
- Authors
- Leadbeater, N. E., & Torenius, H. M.
- Venue
- The Journal of Organic Chemistry
- Publisher
- American Chemical Society (ACS)
- Published
- 2002-04-09
- Volume
- 67
- Issue
- 9
- Pages
- 3145-3148
- ISSN
- 0022-3263 (ISSN-L)
- 1520-6904
- OpenAlex
- W2067918016
- Cited by
- 284
- References
- 1
- FWCI
- 12.96
- Type
- journal article
- Language
- en
- Open access
- closed
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Contains information from the Semantic Scholar Academic Graph Datasets, made available under the ODC Attribution License (ODC-BY 1.0).
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