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Cited by 274

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High-Yield Purification Process of Singlewalled Carbon Nanotubes

Moon, Jeong-Mi, An, Kay Hyeok, Lee, Young Hee, Park, Young Soo, Bae, Dong Jae, Park, Gyeong-Su·2001·The Journal of Physical Chemistry B

Abstract

Reproducible high-yield purification process of singlewalled carbon nanotubes was developed by combining two-step processes of thermal annealing in air and acid treatment. The process involves the thermal annealing in air with the powders rotated at temperatures of 470 °C for 50 min, which burns out the carbonaceous particles, and an acid treatment with HCl for 24 h, which etches away the catalytic metals. Control of the annealing temperature and rotation of the sample are crucial for high yield. Our reproducible optimal purification process provides a total yield of about 25 ∼ 30 wt % with less than 1 wt % of transition metals, which was confirmed by the thermogravimetric analysis. Bundling and length control depending on the different acid treatments will be further discussed.

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Metadata

Authors
Moon, J.-M., An, K. H., Lee, Y. H., Park, Y. S., Bae, D. J., & Park, G.-S.
Venue
The Journal of Physical Chemistry B
Published
2001-05-26
Volume
105
Issue
24
Pages
5677-5681
ISSN
  • 1520-5207 (ISSN-L)
  • 1520-6106
OpenAlex
W1984250391
Cited by
274
References
0
FWCI
11.05
Type
journal article
Language
en
Open access
closed

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Contains information from the Semantic Scholar Academic Graph Datasets, made available under the ODC Attribution License (ODC-BY 1.0).

Semantic Scholar’s data is described in: Kinney, R., et al. (2023). The Semantic Scholar Open Data Platform. arXiv:2301.10140.