The DOI matches its Crossref record; 1 of the 1 references it cites were found in a registry or an index.
ZnO Nanocrystals by a Non-hydrolytic Route: Synthesis and Characterization
Abstract
We report a novel, non-hydrolytic route to ZnO nanocrystals by means of thermal decomposition of zinc acetate (ZnAc 2 ) in alkylamines, in the presence of tert -butylphosphonic acid (TBPA). The slow heating of an alkylamine/TBPA/ZnAc 2 mixture is a simple, safe, and scalable approach to synthesize ZnO nanocrystals from handy chemicals. The obtained ZnO nanocrystals were characterized by UV−vis absorption, photoluminescence (PL) and infrared (FT-IR) spectroscopies, and by X-ray diffraction (XRD) and transmission electron microscopy (TEM). The growth of ZnO particles in the nanoscopic regime and their final size were governed by the TBPA/ZnAc 2 molar ratio in the reaction mixtures. The various roles played by TBPA in the conditions of the synthesis are discussed on the basis of the experimental evidence. The presented synthetic approach provides a unique tool for designing the synthesis of ZnO crystals of a desired size in the nanoscale regime and can be potentially extended to other nanoscale materials.
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Cites
Synthesis of TiO2 Nanocrystals by Nonhydrolytic Solution-Based Reactions
Trentler, T. J., Denler, T. E., Bertone, J. F., Agrawal, A., & Colvin, V. L. (1999) · Journal of the American Chemical Society · doi:10.1021/ja983361b · Cited by 382
Cited by
Toxicity and Environmental Risks of Nanomaterials: Challenges and Future Needs
RAY, P. C., YU, H., & FU, P. P. (2009) · Journal of Environmental Science and Health, Part C · doi:10.1080/10590500802708267 · Cited by 936
Zeng, H., Cai, W., Li, Y., Hu, J., & Liu, P. (2005) · The Journal of Physical Chemistry B · doi:10.1021/jp052258n · Cited by 384
Comparelli, R., Fanizza, E., Curri, M. L., Cozzoli, P. D., Mascolo, G., & Agostiano, A. (2005) · Applied Catalysis B: Environmental · doi:10.1016/j.apcatb.2005.02.013 · Cited by 300
Self-citationMutin, P. H., & Vioux, A. (2009) · Chemistry of Materials · doi:10.1021/cm802348c · Cited by 296
Joo, J., Kwon, S. G., Yu, J. H., & Hyeon, T. (2005) · Advanced Materials · doi:10.1002/adma.200402109 · Cited by 277
Metadata
- Authors
- Cozzoli, P. D., Curri, M. L., Agostiano, A., Leo, G., & Lomascolo, M.
- Venue
- The Journal of Physical Chemistry B
- Publisher
- American Chemical Society (ACS)
- Published
- 2003-04-24
- Volume
- 107
- Issue
- 20
- Pages
- 4756-4762
- ISSN
- 1520-5207 (ISSN-L)
- 1520-6106
- OpenAlex
- W2950678065
- Cited by
- 218
- References
- 1
- FWCI
- 12.29
- Type
- journal article
- Language
- en
- Open access
- closed
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- Cozzoli, P. D., Curri, M. L., Agostiano, A., Leo, G., & Lomascolo, M. (2003). ZnO Nanocrystals by a Non-hydrolytic Route: Synthesis and Characterization. The Journal of Physical Chemistry B. https://doi.org/10.1021/jp027533%2B
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Contains information from the Semantic Scholar Academic Graph Datasets, made available under the ODC Attribution License (ODC-BY 1.0).
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