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Preparation, Characterization, and Photoactivity of Polycrystalline Nanostructured TiO2 Catalysts
Abstract
Various preparations of nanostructured TiO 2 starting from Ti(iso-OC 3 H 7 ) 4 or TiCl 4 are reported. The samples were characterized by X-ray diffractometry, specific surface area and porosity determinations, scanning and transmission electron microscopy, and diffuse reflectance spectroscopy. 4-Nitrophenol photodegradation in aqueous medium was employed as a probe reaction to test the photoactivity of the catalysts. The photoactivity of some samples derived from Ti(iso-OC 3 H 7 ) 4 was found comparable with that of commercial powders. Calcination after the hydrolysis process was necessary to achieve crystallization of the particles before using them as photocatalysts for the reaction studied. The samples deriving from TiCl 4 were the most photoactive among the home-prepared catalysts, and neither filtration nor calcination was needed to obtain a highly photoactive anatase phase.
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Cites
Titanium dioxide aerogels for photocatalytic decontamination of aquatic environments
Dagan, G., & Tomkiewicz, M. (1993) · The Journal of Physical Chemistry · doi:10.1021/j100151a001 · Cited by 284
Cited by
Photoinduced reactivity of titanium dioxide
CARP, O. (2004) · Progress in Solid State Chemistry · doi:10.1016/j.progsolidstchem.2004.08.001 · Cited by 4,566
Synthesis of Square Bi2WO6 Nanoplates as High-Activity Visible-Light-Driven Photocatalysts
Zhang, C., & Zhu, Y. (2005) · Chemistry of Materials · doi:10.1021/cm0501517 · Cited by 912
Wang, X., Liu, Y., Hu, Z., Chen, Y., Liu, W., & Zhao, G. (2009) · Journal of Hazardous Materials · doi:10.1016/j.jhazmat.2009.04.058 · Cited by 198
Metadata
- Authors
- Addamo, M., Augugliaro, V., Di Paola, A., García-López, E., Loddo, V., Marcì, G., Molinari, R., Palmisano, L., & Schiavello, M.
- Venue
- The Journal of Physical Chemistry B
- Publisher
- American Chemical Society (ACS)
- Published
- 2004-02-11
- Volume
- 108
- Issue
- 10
- Pages
- 3303-3310
- ISSN
- 1520-5207 (ISSN-L)
- 1520-6106
- OpenAlex
- W2950141338
- Cited by
- 176
- References
- 1
- FWCI
- 7.82
- Type
- journal article
- Language
- en
- Open access
- closed
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- Addamo, M., Augugliaro, V., Di Paola, A., García-López, E., Loddo, V., Marcì, G., Molinari, R., Palmisano, L., & Schiavello, M. (2004). Preparation, Characterization, and Photoactivity of Polycrystalline Nanostructured TiO2 Catalysts. The Journal of Physical Chemistry B. https://doi.org/10.1021/jp0312924
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