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Reversible Storage of Molecular Hydrogen by Sorption into Multilayered TiO2 Nanotubes
Abstract
The sorption of hydrogen between the layers of the multilayered wall of nanotubular TiO2 was studied in the temperature range of -195 to 200 degrees C and at pressures of 0 to 6 bar. Hydrogen can intercalate between layers in the walls of TiO2 nanotubes forming host-guest compounds TiO2 x xH2, where x < or = 1.5 and decreases at higher temperatures. The rate of hydrogen incorporation increases with temperature and the characteristic time for hydrogen sorption in TiO2 nanotubes is several hours at 100 degrees C. The rate of intercalate formation is limited by the diffusion of molecular hydrogen inside the multilayered walls of the TiO2 nanotube. 1H NMR-MAS and XRD data confirm the incorporation of hydrogen between the layers in the walls of TiO2 nanotubes. The nature and possible applications of the observed intercalates are considered.
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Alternative energy technologies
Dresselhaus, M. S., & Thomas, I. L. (2001) · Nature · doi:10.1038/35104599 · Cited by 4,894
Cited by
Metal hydride materials for solid hydrogen storage: A review
SAKINTUNA, B., LAMARIDARKRIM, F., & HIRSCHER, M. (2007) · International Journal of Hydrogen Energy · doi:10.1016/j.ijhydene.2006.11.022 · Cited by 3,715
Zheng, Z., Huang, B., Lu, J., Wang, Z., Qin, X., Zhang, X., Dai, Y., & Whangbo, M.-H. (2012) · Chemical Communications · doi:10.1039/c2cc32220j · Cited by 313
Metadata
- Authors
- Bavykin, D. V., Lapkin, A. A., Plucinski, P. K., Friedrich, J. M., & Walsh, F. C.
- Venue
- The Journal of Physical Chemistry B
- Publisher
- American Chemical Society (ACS)
- Published
- 2005-09-21
- Volume
- 109
- Issue
- 41
- Pages
- 19422-19427
- ISSN
- 1520-5207 (ISSN-L)
- 1520-6106
- OpenAlex
- W2003317862
- Cited by
- 225
- References
- 1
- FWCI
- 7.05
- Type
- journal article
- Language
- en
- Open access
- closed
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- Bavykin, D. V., Lapkin, A. A., Plucinski, P. K., Friedrich, J. M., & Walsh, F. C. (2005). Reversible Storage of Molecular Hydrogen by Sorption into Multilayered TiO2 Nanotubes. The Journal of Physical Chemistry B. https://doi.org/10.1021/jp0536394
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