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Solvent-Assisted Thermal Reduction of Graphite Oxide
Abstract
The thermal behavior of graphite oxide (GO) is essential to study and design GO reduction and functionalizion reaction. We provide a detailed description of the thermal reduction of GO dispersed in solvent (H 2 O and dimethylformamide (DMF)) at temperatures of 100 and 150 °C, respectively. The thermal stability and structure change of GO during the thermal treatment were characterized using UV−vis spectroscopy, Raman spectroscopy, X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FTIR), X-ray photoelectron spectroscopy (XPS), and thermogravimetric analysis (TGA). It was found that at temperatures of 100 and 150 °C the carboxylic and carbonyl groups decomposed. GO dispersed in H 2 O and DMF at temperatures of 100 and 150 °C exhibited increased rates of reduction than in dry condition. Moreover, the reduction rate was found to be highly dependent on the solvent used. At 150 °C, DMF accelerates the GO reduction rate significantly, while dimethyl sulfoxide (DMSO) has less acceleration effect. However, ethylene glycol (EG) reduces the reduction rate compared to dry conditions. The solvent−GO interaction, including polar−polar interaction and hydrogen bonding, was discussed as one possible reason for the solvent-dependent reduction.
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Superior Thermal Conductivity of Single-Layer Graphene
Balandin, A. A., Ghosh, S., Bao, W., Calizo, I., Teweldebrhan, D., Miao, F., & Lau, C. N. (2008) · Nano Letters · doi:10.1021/nl0731872 · Cited by 13,823
Ni(OH) 2 Nanoplates Grown on Graphene as Advanced Electrochemical Pseudocapacitor Materials
Wang, H., Casalongue, H. S., Liang, Y., & Dai, H. (2010) · Journal of the American Chemical Society · doi:10.1021/ja102267j · Cited by 2,042
Metadata
- Authors
- Lin, Z., Yao, Y., Li, Z., Liu, Y., Li, Z., & Wong, C.-P.
- Venue
- The Journal of Physical Chemistry C
- Publisher
- American Chemical Society (ACS)
- Published
- 2010-08-19
- Volume
- 114
- Issue
- 35
- Pages
- 14819-14825
- ISSN
- 1932-7447 (ISSN-L)
- 1932-7455
- OpenAlex
- W2031014750
- Cited by
- 300
- References
- 2
- FWCI
- 13.13
- Type
- journal article
- Language
- en
- Open access
- closed
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- Lin, Z., Yao, Y., Li, Z., Liu, Y., Li, Z., & Wong, C.-P. (2010). Solvent-Assisted Thermal Reduction of Graphite Oxide. The Journal of Physical Chemistry C. https://doi.org/10.1021/jp1049843
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