The DOI matches its Crossref record; 26 of the 26 references it cites were found in a registry or an index.
Electron–Water Interactions and Implications for Liquid Cell Electron Microscopy
Abstract
Liquid cell electron microscopy enables direct in situ imaging of processes in liquids and objects suspended in liquids with nanoscale resolution. However, the irradiating electrons affect the chemistry of the suspending medium, typically an aqueous solution, producing molecular and radical products such as hydrogen, oxygen, and hydrated (solvated) electrons. These may impact the imaged structures and phenomena. A good understanding of the interactions between the electrons and the irradiated medium is necessary to correctly interpret experiments, minimize artifacts, and take advantage of the irradiation. We predict the composition of water subjected to electron irradiation in the electron microscope. We reinterpret available experimental data, such as beam-induced variations in pH and colloid aggregation, in light of our predictions and show new observations of crystallization and etching as functions of dose rate, resolving conflicting reports in the scientific literature. We make our computer code available to readers. Our predictive model is useful for designing experiments that minimize unwanted beam effects, extending liquid cell microscopy to new applications, taking advantage of beam effects for nanomanufacturing such as the patterning of nanostructures, and correctly interpreting experimental observations. Additionally, our results indicate that liquid cells provide a new tool to study radiolysis effects on materials and processes.
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Cites
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Direction-Specific Interactions Control Crystal Growth by Oriented Attachment
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Self-citationIntroduction to radiation chemistry
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Electrocatalysis in Alkaline Media and Alkaline Membrane-Based Energy Technologies
Yang, Y., Peltier, C. R., Zeng, R., Schimmenti, R., Li, Q., Huang, X., Yan, Z., Potsi, G., Selhorst, R., Lu, X., et al. (2022) · Chemical Reviews · doi:10.1021/acs.chemrev.1c00331 · Cited by 544
Liquid–liquid phase separation during amphiphilic self-assembly
Ianiro, A., Wu, H., van Rijt, M. M. J., Vena, M. P., Keizer, A. D. A., Esteves, A. C. C., Tuinier, R., Friedrich, H., Sommerdijk, N. A. J. M., & Patterson, J. P. (2019) · Nature Chemistry · doi:10.1038/s41557-019-0210-4 · Cited by 283
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Metadata
- Authors
- Schneider, N. M., Norton, M. M., Mendel, B. J., Grogan, J. M., Ross, F. M., & Bau, H. H.
- Venue
- The Journal of Physical Chemistry C
- Publisher
- American Chemical Society (ACS)
- Published
- 2014-09-11
- Volume
- 118
- Issue
- 38
- Pages
- 22373-22382
- ISSN
- 1932-7447 (ISSN-L)
- 1932-7455
- OpenAlex
- W2031004957
- Cited by
- 654
- References
- 26
- FWCI
- 23.39
- Type
- journal article
- Language
- en
- Open access
- closed
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- Schneider, N. M., Norton, M. M., Mendel, B. J., Grogan, J. M., Ross, F. M., & Bau, H. H. (2014). Electron–Water Interactions and Implications for Liquid Cell Electron Microscopy. The Journal of Physical Chemistry C. https://doi.org/10.1021/jp507400n
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Contains information from the Semantic Scholar Academic Graph Datasets, made available under the ODC Attribution License (ODC-BY 1.0).
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