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Large Scale CVD Synthesis of Single-Walled Carbon Nanotubes
Abstract
The synthesis of bulk amounts of high quality single-walled carbon nanotubes (SWNTs) is accomplished by optimizing the chemical compositions and textural properties of the catalyst material used in the chemical vapor deposition (CVD) of methane. A series of catalysts are derived by systematically varying the catalytic metal compounds and support materials. The optimized catalysts consist of Fe/Mo bimetallic species supported on a novel silica−alumina multicomponent material. The high SWNT yielding catalyst exhibits high surface-area and large mesopore volume at elevated temperatures. Gram quantities of SWNT materials have been synthesized in ∼0.5 h using the optimized catalyst material. The nanotube material consists of individual and bundled SWNTs that are free of defects and amorphous carbon coating. This work represents a step forward toward obtaining kilogram scale perfect SWNT materials via simple CVD routes.
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Metadata
- Authors
- Cassell, A. M., Raymakers, J. A., Kong, J., & Dai, H.
- Venue
- The Journal of Physical Chemistry B
- Publisher
- American Chemical Society (ACS)
- Published
- 1999-07-20
- Volume
- 103
- Issue
- 31
- Pages
- 6484-6492
- ISSN
- 1520-5207 (ISSN-L)
- 1520-6106
- OpenAlex
- W1985588689
- Cited by
- 918
- References
- 1
- FWCI
- 22.59
- Type
- journal article
- Language
- en
- Open access
- closed
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