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Size Distributions of Gold Nanoclusters Studied by Liquid Chromatography
Open accessAbstract
We report high-pressure liquid chromatography (HPLC) and transmission electron microscopy (TEM) studies of the size distributions of nanosize gold clusters dispersed in organic solvents. These metal clusters are synthesized in inverse micelles at room temperature, and those investigated range in diameter from 1 to 10 nm. HPLC is sensitive enough to discern changes in hydrodynamic volume corresponding to only 2 carbon atoms of the passivating agent or metal core size changes of less than 4 Å. We have determined for the first time how the total cluster volume (metal core + passivating organic shell) changes with the size of the passivating agent.
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Cited by
Negishi, Y., Nobusada, K., & Tsukuda, T. (2005) · Journal of the American Chemical Society · doi:10.1021/ja042218h · Cited by 1,646
Sub-nanometre sized metal clusters: from synthetic challenges to the unique property discoveries
Lu, Y., & Chen, W. (2012) · Chemical Society Reviews · doi:10.1039/c2cs15325d · Cited by 1,152
Synthesis, structure and properties of metal nanoclusters
Wilcoxon, J. P., & Abrams, B. L. (2006) · Chemical Society Reviews · doi:10.1039/b517312b · Cited by 760
Self-citationThe use of nanoparticles in electroanalysis: a review
Welch, C. M., & Compton, R. G. (2006) · Analytical and Bioanalytical Chemistry · doi:10.1007/s00216-005-0230-3 · Cited by 759
Charge Transport in Nanoparticle Assemblies
Zabet-Khosousi, A., & Dhirani, A.-A. (2008) · Chemical Reviews · doi:10.1021/cr0680134 · Cited by 503
Metadata
- Authors
- Wilcoxon, J. P., Martin, J. E., & Provencio, P.
- Venue
- Langmuir
- Publisher
- American Chemical Society (ACS)
- Published
- 2000-10-31
- Volume
- 16
- Issue
- 25
- Pages
- 9912-9920
- ISSN
- 0743-7463 (ISSN-L)
- 1520-5827
- OpenAlex
- W2090452166
- Cited by
- 168
- References
- 0
- FWCI
- 4.25
- Type
- journal article
- Language
- en
- Open access
- green
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