The DOI matches its Crossref record; 2 of the 2 references it cites were found in a registry or an index.
Birefringent Glassy Phase of a Cellulose Microcrystal Suspension
Abstract
We prepared a stable and highly viscous suspension of cellulose microcrystals by postsulfating the HCl-hydrolyzed cellulose microcrystals. The neutralized suspension was isotropic and showed flow birefringence at low solid content (ca. <1%). At a solid content of approximately 2−3%, the suspension was still flowing but showed intricate birefringent patterns, which remained after the flow had ceased. At high solid content (7.1%), the suspension became too viscous to flow and showed a frozen-in birefringent pattern with a microscopic crosshatch texture. These features show that this postsulfated suspension forms a “birefringent glassy phase”, similar to that observed for a boehmite rod suspension, being distinctly different from the behavior of the suspension prepared by direct hydrolysis of cellulose with concentrated sulfuric acid.
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Citations
Cites
Effect of microcrystallite preparation conditions on the formation of colloid crystals of cellulose
DONG, X. M., REVOL, J.-F., & GRAY, D. G. (1998) · Cellulose · doi:10.1023/a:1009260511939 · Cited by 1,032
Araki, J., Wada, M., Kuga, S., & Okano, T. (1998) · Colloids and Surfaces A: Physicochemical and Engineering Aspects · doi:10.1016/s0927-7757(98)00404-x · Cited by 769
Self-citation
Cited by
Cellulose nanomaterials review: structure, properties and nanocomposites
Moon, R. J., Martini, A., Nairn, J., Simonsen, J., & Youngblood, J. (2011) · Chemical Society Reviews · doi:10.1039/c0cs00108b · Cited by 6,756
Cellulose nanocrystals: chemistry, self-assembly, and applications
Habibi, Y., Lucia, L. A., & Rojas, O. J. (2010) · Chemical Reviews · doi:10.1021/cr900339w · Cited by 5,980
Beck-Candanedo, S., Roman, M., & Gray, D. G. (2005) · Biomacromolecules · doi:10.1021/bm049300p · Cited by 1,588
Wood-Derived Materials for Green Electronics, Biological Devices, and Energy Applications
Zhu, H., Luo, W., Ciesielski, P. N., Fang, Z., Zhu, J. Y., Henriksson, G., Himmel, M. E., & Hu, L. (2016) · Chemical Reviews · doi:10.1021/acs.chemrev.6b00225 · Cited by 1,532
Optimization of the isolation of nanocrystals from microcrystalline cellulose by acid hydrolysis
Bondeson, D., Mathew, A., & Oksman, K. (2006) · Cellulose · doi:10.1007/s10570-006-9061-4 · Cited by 1,372
Metadata
- Authors
- Araki, J., Wada, M., Kuga, S., & Okano, T.
- Venue
- Langmuir
- Publisher
- American Chemical Society (ACS)
- Published
- 2000-02-11
- Volume
- 16
- Issue
- 6
- Pages
- 2413-2415
- ISSN
- 0743-7463 (ISSN-L)
- 1520-5827
- OpenAlex
- W2042307844
- Cited by
- 235
- References
- 2
- FWCI
- 1.60
- Type
- journal article
- Language
- en
- Open access
- closed
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