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Fibrillar Structure of Nafion: Matching Fourier and Real Space Studies of Corresponding Films and Solutions
Abstract
Using both scattering and microscopy techniques, we have characterized the complex Nafion structure over a large range of length scales. Analysis of experimental data from dry membrane to aqueous dispersion suggests an intrinsic fibrillar structure. The fibrils correspond to elongated polymeric aggregates surrounded with the ionic charges. In the Nafion membrane, the fibrils are entangled and collapsed with a degree of orientation at the mesoscopic scale. Upon swelling and temperature treatment, these aggregates are hydrated and dispersed in a colloidal suspension.
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Cites
On the development of proton conducting polymer membranes for hydrogen and methanol fuel cells
Kreuer, K. D. (2001) · Journal of Membrane Science · doi:10.1016/s0376-7388(00)00632-3 · Cited by 2,969
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Kusoglu, A., & Weber, A. Z. (2017) · Chemical Reviews · doi:10.1021/acs.chemrev.6b00159 · Cited by 2,432
Parallel cylindrical water nanochannels in Nafion fuel-cell membranes
Schmidt-Rohr, K., & Chen, Q. (2008) · Nature Materials · doi:10.1038/nmat2074 · Cited by 1,371
Water transport in polymer electrolyte membrane fuel cells
Jiao, K., & Li, X. (2011) · Progress in Energy and Combustion Science · doi:10.1016/j.pecs.2010.06.002 · Cited by 1,086
Structure‐Morphology‐Property Relationships of Non‐Perfluorinated Proton‐Conducting Membranes
Peckham, T. J., & Holdcroft, S. (2010) · Advanced Materials · doi:10.1002/adma.201001164 · Cited by 622
Stable Cycling of Lithium Metal Batteries Using High Transference Number Electrolytes
Lu, Y., Tikekar, M., Mohanty, R., Hendrickson, K., Ma, L., & Archer, L. A. (2015) · Advanced Energy Materials · doi:10.1002/aenm.201402073 · Cited by 377
Metadata
- Authors
- Rubatat, L., Gebel, G., & Diat, O.
- Venue
- Macromolecules
- Publisher
- American Chemical Society (ACS)
- Published
- 2004-09-08
- Volume
- 37
- Issue
- 20
- Pages
- 7772-7783
- ISSN
- 0024-9297 (ISSN-L)
- 1520-5835
- OpenAlex
- W1966798416
- Cited by
- 376
- References
- 1
- FWCI
- 15.37
- Type
- journal article
- Language
- en
- Open access
- closed
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- Rubatat, L., Gebel, G., & Diat, O. (2004). Fibrillar Structure of Nafion: Matching Fourier and Real Space Studies of Corresponding Films and Solutions. Macromolecules. https://doi.org/10.1021/ma049683j
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Contains information from the Semantic Scholar Academic Graph Datasets, made available under the ODC Attribution License (ODC-BY 1.0).
Semantic Scholar’s data is described in: Kinney, R., et al. (2023). The Semantic Scholar Open Data Platform. arXiv:2301.10140.
