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Purity Evaluation of As-Prepared Single-Walled Carbon Nanotube Soot by Use of Solution-Phase Near-IR Spectroscopy
Abstract
We report a rapid, quantitative procedure for the evaluation of the carbonaceous purity of bulk quantities of as-prepared single-walled carbon nanotube (SWNT) soot by the utilization of solution-phase near-IR spectroscopy. The procedure starts with two steps of homogenization followed by solution/dispersion spectroscopy of a representative part of the bulk sample. The purity is evaluated against a reference sample by utilizing the region of the second interband transition (S 22 ) for semiconducting SWNTs. The procedure is found to be capable of reliably analyzing the carbonaceous purity of a 10-g batch of SWNTs produced by the electric arc discharge method to within 3%.
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Metadata
- Authors
- Itkis, M. E., Perea, D. E., Niyogi, S., Rickard, S. M., Hamon, M. A., Hu, H., Zhao, B., & Haddon, R. C.
- Venue
- Nano Letters
- Publisher
- American Chemical Society (ACS)
- Published
- 2003-01-22
- Volume
- 3
- Issue
- 3
- Pages
- 309-314
- ISSN
- 1530-6984 (ISSN-L)
- 1530-6992
- OpenAlex
- W2076342521
- Cited by
- 339
- References
- 0
- FWCI
- 14.62
- Type
- journal article
- Language
- en
- Open access
- closed
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