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Kinetics of Diazonium Functionalization of Chemically Converted Graphene Nanoribbons
Abstract
We demonstrate that graphene nanoribbons (GNRs) produced by the oxidative unzipping of carbon nanotubes can be chemically functionalized by diazonium salts. We show that functional groups form a thin layer on a GNR and modify its electrical properties. The kinetics of the functionalization can be monitored by probing the electrical properties of GNRs, either in vacuum after the grafting, or in situ in the solution. We derive a simple kinetics model that describes the change in the electrical properties of GNRs. The reaction of GNRs with 4-nitrobenzene diazonium tetrafluoroborate is reasonably fast, such that >60% of the maximum change in the electrical properties is observed after less than 5 min of grafting at room temperature.
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Cites
Graphene: Status and Prospects
Geim, A. K. (2009) · Science · doi:10.1126/science.1158877 · Cited by 13,942
Lower-Defect Graphene Oxide Nanoribbons from Multiwalled Carbon Nanotubes
Higginbotham, A. L., Kosynkin, D. V., Sinitskii, A., Sun, Z., & Tour, J. M. (2010) · ACS Nano · doi:10.1021/nn100118m · Cited by 585
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Cited by
Synthesis and characterization of sulfophenyl-functionalized reduced graphene oxide sheets
Ossonon, B. D., & Bélanger, D. (2017) · RSC Advances · doi:10.1039/c6ra28311j · Cited by 496
Synthesis of graphene materials by electrochemical exfoliation: Recent progress and future potential
Liu, F., Wang, C., Sui, X., Riaz, M. A., Xu, M., Wei, L., & Chen, Y. (2019) · Carbon Energy · doi:10.1002/cey2.14 · Cited by 407
Metadata
- Authors
- Sinitskii, A., Dimiev, A., Corley, D. A., Fursina, A. A., Kosynkin, D. V., & Tour, J. M.
- Venue
- ACS Nano
- Publisher
- American Chemical Society (ACS)
- Published
- 2010-03-26
- Volume
- 4
- Issue
- 4
- Pages
- 1949-1954
- ISSN
- 1936-0851 (ISSN-L)
- 1936-086X
- OpenAlex
- W1982506260
- Cited by
- 367
- References
- 2
- FWCI
- 11.58
- Type
- journal article
- Language
- en
- Open access
- closed
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