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Structural isomerism in gold nanoparticles revealed by X-ray crystallography
Open accessAbstract
Revealing structural isomerism in nanoparticles using single-crystal X-ray crystallography remains a largely unresolved task, although it has been theoretically predicted with some experimental clues. Here we report a pair of structural isomers, Au 38T and Au 38Q, as evidenced using electrospray ionization mass spectrometry, X-ray photoelectron spectroscopy, thermogravimetric analysis and indisputable single-crystal X-ray crystallography. The two isomers show different optical and catalytic properties, and differences in stability. In addition, the less stable Au 38T can be irreversibly transformed to the more stable Au 38Q at 50 °C in toluene. This work may represent an important advance in revealing structural isomerism at the nanoscale.
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Lu, Y., & Chen, W. (2012) · Chemical Society Reviews · doi:10.1039/c2cs15325d · Cited by 1,152
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Self-citationNonclassical nucleation and growth of inorganic nanoparticles
Lee, J., Yang, J., Kwon, S. G., & Hyeon, T. (2016) · Nature Reviews Materials · doi:10.1038/natrevmats.2016.34 · Cited by 530
Self-citationUnraveling the long-pursued Au 144 structure by x-ray crystallography
Yan, N., Xia, N., Liao, L., Zhu, M., Jin, F., Jin, R., & Wu, Z. (2018) · Science Advances · doi:10.1126/sciadv.aat7259 · Cited by 353
Self-citationChemical Flexibility of Atomically Precise Metal Clusters
Li, S., Li, N.-N., Dong, X.-Y., Zang, S.-Q., & Mak, T. C. W. (2024) · Chemical Reviews · doi:10.1021/acs.chemrev.3c00896 · Cited by 280
Metadata
- Authors
- Tian, S., Li, Y.-Z., Li, M.-B., Yuan, J., Yang, J., Wu, Z., & Jin, R.
- Venue
- Nature Communications
- Published
- 2015-10-20
- Volume
- 6
- Issue
- 1
- Pages
- 10012-10012
- ISSN
- 2041-1723 (ISSN-L)
- OpenAlex
- W1806907900
- Cited by
- 329
- References
- 1
- FWCI
- 12.79
- Type
- journal article
- Language
- en
- Open access
- gold
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- Tian, S., Li, Y.-Z., Li, M.-B., Yuan, J., Yang, J., Wu, Z., & Jin, R. (2015). Structural isomerism in gold nanoparticles revealed by X-ray crystallography. Nature Communications. https://doi.org/10.1038/ncomms9667
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