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Synthesis of brookite TiO2 nanoparticles by thermolysis of TiCl4 in strongly acidic aqueous media
Abstract
Nanometric particles of titania, brookite and rutile polymorphs were synthesised by thermolysis of TiCl4 in concentrated HCl solutions. The Cl∶Ti molar ratio seems to be the key factor in determining the crystalline phases and their relative proportions as well as the particle size and a large proportion of brookite can be obtained under specific conditions. The complex Ti(OH)2(Cl)2(OH2)2 seems to be the precursor of the brookite phase. The presence of chloride ions is also necessary to stabilise brookite in suspension. Depending on the acidity and the ageing conditions, different morphologies of brookite nanoparticles are obtained, namely spheroidal particles or platelets. Stable sols of pure brookite are obtained by peptization of the solid phase.
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Cites
Electrochemical Photolysis of Water at a Semiconductor Electrode
FUJISHIMA, A., & HONDA, K. (1972) · Nature · doi:10.1038/238037a0 · Cited by 34,169
A low-cost, high-efficiency solar cell based on dye-sensitized colloidal TiO2 films
O'Regan, B., & Grätzel, M. (1991) · Nature · doi:10.1038/353737a0 · Cited by 28,599
Cited by
Liu, B., & Aydil, E. S. (2009) · Journal of the American Chemical Society · doi:10.1021/ja8078972 · Cited by 2,381
Virtual screening of inorganic materials synthesis parameters with deep learning
Kim, E., Huang, K., Jegelka, S., & Olivetti, E. (2017) · npj Computational Materials · doi:10.1038/s41524-017-0055-6 · Cited by 190
Pori, P., Vilčnik, A., Petrič, M., Sever Škapin, A., Mihelčič, M., Šurca Vuk, A., Novak, U., & Orel, B. (2016) · Applied Surface Science · doi:10.1016/j.apsusc.2016.03.065 · Cited by 41
Metadata
- Authors
- Pottier, A., Chanéac, C., Tronc, E., Mazerolles, L., & Jolivet, J.-P.
- Venue
- Journal of Materials Chemistry
- Publisher
- Royal Society of Chemistry (RSC)
- Published
- 2001
- Volume
- 11
- Issue
- 4
- Pages
- 1116-1121
- ISSN
- 0959-9428 (ISSN-L)
- 1364-5501
- OpenAlex
- W2083833748
- Cited by
- 402
- References
- 2
- FWCI
- 10.67
- Type
- journal article
- Language
- en
- Open access
- closed
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- Pottier, A., Chanéac, C., Tronc, E., Mazerolles, L., & Jolivet, J.-P. (2001). Synthesis of brookite TiO2 nanoparticles by thermolysis of TiCl4 in strongly acidic aqueous media. Journal of Materials Chemistry. https://doi.org/10.1039/b100435m
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