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Microporosity and connections between pores in SBA-15 mesostructured silicas as a function of the temperature of synthesis
Abstract
Imaging of the platinum replica of the porous structure and low-pressure argon adsorption allowed us to elucidate the complicated porous structure of SBA-15. These techniques enabled us to draw a coherent picture of the evolution of the SBA-15 precursor mesophase as a function of the synthesis temperature. TEM of the platinum replicas has been unable to show bridges between the structural mesopores of SBA-15 synthesized at low temperature, whereas mesoporous bridges are clearly observed for samples formed at higher temperature. Argon adsorption has evidenced the ultramicroporosity of the materials formed at low temperature, as well as its evolution to secondary porosity with diameters greater than 1.5 nm under more severe hydrothermal treatment.
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Citations
Cites
Characterization of the porous structure of sba-15
Kruk, M., Jaroniec, M., Ko, C. H., & Ryoo, R. (2000) · Chemistry of Materials · doi:10.1021/cm000164e · Cited by 1,409
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Cited by
On the controllable soft-templating approach to mesoporous silicates
Wan, Y., & Zhao (2007) · Chemical Reviews · doi:10.1021/cr068020s · Cited by 2,371
Ordered mesoporous materials in catalysis
Taguchi, A., & Schüth, F. (2005) · Microporous and Mesoporous Materials · doi:10.1016/j.micromeso.2004.06.030 · Cited by 2,119
Kim, T.-W., Kleitz, F., Paul, B., & Ryoo, R. (2005) · Journal of the American Chemical Society · doi:10.1021/ja042601m · Cited by 733
Self-citationZhang, S., Zhang, J., Zhang, Y., & Deng, Y. (2017) · Chemical Reviews · doi:10.1021/acs.chemrev.6b00509 · Cited by 659
Metadata
- Authors
- Galarneau, A., Cambon, H., Di Renzo, F., Ryoo, R., Choi, M., & Fajula, F.
- Venue
- New Journal of Chemistry
- Publisher
- Royal Society of Chemistry (RSC)
- Published
- 2002-11-28
- Volume
- 27
- Issue
- 1
- Pages
- 73-79
- ISSN
- 0398-9836 (ISSN-L)
- 1144-0546
- 1369-9261
- OpenAlex
- W2139993551
- Cited by
- 559
- References
- 1
- FWCI
- 12.63
- Type
- journal article
- Language
- en
- Open access
- closed
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- Galarneau, A., Cambon, H., Di Renzo, F., Ryoo, R., Choi, M., & Fajula, F. (2003). Microporosity and connections between pores in SBA-15 mesostructured silicas as a function of the temperature of synthesis. New Journal of Chemistry. https://doi.org/10.1039/b207378c
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