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Independent verification of the saturation hydrogen uptake in MOF-177 and establishment of a benchmark for hydrogen adsorption in metal–organic frameworks
Abstract
Hydrogen isotherms for MOF-177, Zn4O(1,3,5-benzenetribenzoate)2, crystals were independently measured by volumetric and gravimetric methods at 77 K to confirm its hydrogen uptake capacity and to establish the importance of calibrating gas adsorption instrumentation prior to evaluating H2 storage capacities. Reproducibility of hydrogen adsorption experiments is important because non-systematic errors in measurements can easily occur leading to erroneous reports of capacities. The surface excess weight percentage of hydrogen uptake in MOF-177 samples is 7.5 wt% at 70 bar, which corresponds to an absolute adsorbed amount of 11 wt%. These values are in agreement with our previous report and with those found independently by Southwest Research Institute. Considering its well-known structure and its significant H2 uptake properties, we believe MOF-177 is an excellent material to serve as a benchmark adsorber.
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Cited by
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Xie, Y., Wang, T.-T., Liu, X.-H., Zou, K., & Deng, W.-Q. (2013) · Nature Communications · doi:10.1038/ncomms2960 · Cited by 772
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Dalebrook, A. F., Gan, W., Grasemann, M., Moret, S., & Laurenczy, G. (2013) · Chemical Communications · doi:10.1039/c3cc43836h · Cited by 503
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Metadata
- Authors
- Furukawa, H., Miller, M. A., & Yaghi, O. M.
- Venue
- Journal of Materials Chemistry
- Publisher
- Royal Society of Chemistry (RSC)
- Published
- 2007
- Volume
- 17
- Issue
- 30
- Pages
- 3197
- ISSN
- 0959-9428 (ISSN-L)
- 1364-5501
- OpenAlex
- W1998128953
- Cited by
- 607
- References
- 0
- FWCI
- 38.86
- Type
- journal article
- Language
- en
- Open access
- closed
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- Furukawa, H., Miller, M. A., & Yaghi, O. M. (2007). Independent verification of the saturation hydrogen uptake in MOF-177 and establishment of a benchmark for hydrogen adsorption in metal–organic frameworks. Journal of Materials Chemistry. https://doi.org/10.1039/b703608f
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