The DOI matches its Crossref record; 3 of the 3 references it cites were found in a registry or an index.
Conversion of carbohydrates into 5-hydroxymethylfurfural in highly concentrated low melting mixtures
Abstract
Highly concentrated melt systems consisting of choline chloride (ChCl) and up to 50 wt% of carbohydrates, corresponding to carbohydrate concentrations of 2.9 to 3.1 mol/L, have been used for the conversion of the carbohydrate content into 5-hydroxymethylfurfural (HMF) in the presence of catalysts. Apart from the monosaccharides D-fructose and D-glucose, the disaccharide sucrose and the polyfructan inulin were successfully converted into HMF. The reported conditions with short reaction times at high concentrations may allow for high space-time yields, which may be of interest for the development of efficient continuous processes for the conversion of carbohydrates into HMF. In a preliminary ecological evaluation, the ChCl/D-fructose system is compared to other representative solvents for the synthesis of 5-hydroxymethylfurfural. The melts have an inherent low toxicological impact due to their negligible vapour pressure.
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Cites
Abbott, A. P., Capper, G., Davies, D. L., Rasheed, R. K., & Tambyrajah, V. (2003) · Chemical Communications · doi:10.1039/b210714g · Cited by 5,738
Metal Chlorides in Ionic Liquid Solvents Convert Sugars to 5-Hydroxymethylfurfural
Zhao, H., Holladay, J. E., Brown, H., & Zhang, Z. C. (2007) · Science · doi:10.1126/science.1141199 · Cited by 1,997
Acid-Catalyzed Production of 5-Hydroxymethyl Furfural from d-Fructose in Subcritical Water
Salak Asghari, F., & Yoshida, H. (2006) · Industrial & Engineering Chemistry Research · doi:10.1021/ie051088y · Cited by 500
Cited by
Deep eutectic solvents: syntheses, properties and applications
Zhang, Q., De Oliveira Vigier, K., Royer, S., & Jérôme, F. (2012) · Chemical Society Reviews · doi:10.1039/c2cs35178a · Cited by 4,899
Hydroxymethylfurfural, A Versatile Platform Chemical Made from Renewable Resources
van Putten, R.-J., van der Waal, J. C., de Jong, E., Rasrendra, C. B., Heeres, H. J., & de Vries, J. G. (2013) · Chemical Reviews · doi:10.1021/cr300182k · Cited by 2,886
Gu, Y., & Jérôme, F. (2013) · Chemical Society Reviews · doi:10.1039/c3cs60241a · Cited by 668
Low melting mixtures in organic synthesis–an alternative to ionic liquids?
Ruß, C., & König, B. (2012) · Green Chemistry · doi:10.1039/c2gc36005e · Cited by 654
Self-citationDai, Y., van Spronsen, J., Witkamp, G.-J., Verpoorte, R., & Choi, Y. H. (2013) · Journal of Natural Products · doi:10.1021/np400051w · Cited by 472
Metadata
- Authors
- Ilgen, F., Ott, D., Kralisch, D., Reil, C., Palmberger, A., & König, B.
- Venue
- Green Chemistry
- Publisher
- Royal Society of Chemistry (RSC)
- Published
- 2009
- Volume
- 11
- Issue
- 12
- Pages
- 1948
- ISSN
- 1463-9262 (ISSN-L)
- 1463-9270
- OpenAlex
- W1987707389
- Cited by
- 307
- References
- 3
- FWCI
- 9.51
- Type
- journal article
- Language
- en
- Open access
- closed
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- Ilgen, F., Ott, D., Kralisch, D., Reil, C., Palmberger, A., & König, B. (2009). Conversion of carbohydrates into 5-hydroxymethylfurfural in highly concentrated low melting mixtures. Green Chemistry. https://doi.org/10.1039/b917548m
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