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Microwave-assisted hydrolysis of crystalline cellulose catalyzed by biomass char sulfonic acids
Abstract
The development of an environmentally benign process for the hydrolysis of cellulose into reducing sugars can be one of the key technologies for making full use of cellulosic biomass in the future. Here, a biomass char sulfonic acid (BC-SO3H)-catalyzed hydrolysis of cellulose in water was achieved under microwave irradiation. The BC-SO3H catalysts prepared cheaply from natural bamboo, cotton and starch, showed a much higher turnover number (TON, 1.33-1.73) for this reaction compared to a dilute H2SO4 solution (TON, 0.02), which was likely due to their strong affinity to β-1,4-glycosidic bonds of cellulose. In addition, microwave irradiation played key roles in activating cellulose molecules and strengthening particle collision, which can lead to a remarkable acceleration effect on this heterogeneously catalytic process.
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Citations
Cites
Use of Dinitrosalicylic Acid Reagent for Determination of Reducing Sugar
Miller, G. L. (1959) · Analytical Chemistry · doi:10.1021/ac60147a030 · Cited by 28,963
Cited by
Development of biochar-based functional materials: toward a sustainable platform carbon material
Liu, W.-J., Jiang, H., & Yu, H.-Q. (2015) · Chemical Reviews · doi:10.1021/acs.chemrev.5b00195 · Cited by 1,754
Catalytic conversion of lignocellulosic biomass to fine chemicals and fuels
Zhou, C.-H., Xia, X., Lin, C.-X., Tong, D.-S., & Beltramini, J. (2011) · Chemical Society Reviews · doi:10.1039/c1cs15124j · Cited by 1,420
Hydrolysis of cellulose to glucose by solid acid catalysts
Huang, Y.-B., & Fu, Y. (2013) · Green Chemistry · doi:10.1039/c3gc40136g · Cited by 717
Recent Advances in the Catalytic Conversion of Cellulose
Van de Vyver, S., Geboers, J., Jacobs, P. A., & Sels, B. F. (2011) · ChemCatChem · doi:10.1002/cctc.201000302 · Cited by 567
Hydrolysis of cellulose into glucose over carbons sulfonated at elevated temperatures
Pang, J., Wang, A., Zheng, M., & Zhang, T. (2010) · Chemical Communications · doi:10.1039/c0cc02014a · Cited by 340
Metadata
- Authors
- Wu, Y., Fu, Z., Yin, D., Xu, Q., Liu, F., Lu, C., & Mao, L.
- Venue
- Green Chemistry
- Publisher
- Royal Society of Chemistry (RSC)
- Published
- 2010
- Volume
- 12
- Issue
- 4
- Pages
- 696
- ISSN
- 1463-9262 (ISSN-L)
- 1463-9270
- OpenAlex
- W2080154924
- Cited by
- 265
- References
- 1
- FWCI
- 9.47
- Type
- journal article
- Language
- en
- Open access
- closed
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Contains information from the Semantic Scholar Academic Graph Datasets, made available under the ODC Attribution License (ODC-BY 1.0).
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