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HKUST-1 membranes on porous supports using secondary growth
Abstract
Here we report the synthesis of continuous HKUST-1 membranes on porous supports via the secondary (i.e., seeded) growth method. A new seeding technique (“thermal seeding”) was developed to strongly anchor HKUST-1 seed crystals on porous α-alumina supports. It was found critical to have both organic ligands and copper species in the seed suspension as well as to seed the crystals at elevated temperature. The HKUST-1 seed crystals on the supports were then hydrothermally grown into continuous HKUST-1 films. The formation of cracks and fractures in the films was prevented by controlling the cooling and the drying processes after crystallization. The permeation results of HKUST-1 membranes show moderate separation of hydrogen over other small gas molecules such as carbon dioxide, nitrogen, oxygen, and methane.
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Cites
Metal-organic framework materials as catalysts
Lee, J., Farha, O. K., Roberts, J., Scheidt, K. A., Nguyen, S. T., & Hupp, J. T. (2009) · Chemical Society Reviews · doi:10.1039/b807080f · Cited by 7,969
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Metal–Organic Frameworks for Separations
Li, J.-R., Sculley, J., & Zhou, H.-C. (2012) · Chemical Reviews · doi:10.1021/cr200190s · Cited by 6,323
MOF positioning technology and device fabrication
Falcaro, P., Ricco, R., Doherty, C. M., Liang, K., Hill, A. J., & Styles, M. J. (2014) · Chem. Soc. Rev. · doi:10.1039/c4cs00089g · Cited by 710
Current Status of Metal–Organic Framework Membranes for Gas Separations: Promises and Challenges
Shah, M., McCarthy, M. C., Sachdeva, S., Lee, A. K., & Jeong, H.-K. (2012) · Industrial & Engineering Chemistry Research · doi:10.1021/ie202038m · Cited by 494
Self-citationWang, C.-C., Wang, X., & Liu, W. (2020) · Chemical Engineering Journal · doi:10.1016/j.cej.2019.123601 · Cited by 258
Metadata
- Authors
- Guerrero, V. V., Yoo, Y., McCarthy, M. C., & Jeong, H.-K.
- Venue
- Journal of Materials Chemistry
- Publisher
- Royal Society of Chemistry (RSC)
- Published
- 2010
- Volume
- 20
- Issue
- 19
- Pages
- 3938
- ISSN
- 0959-9428 (ISSN-L)
- 1364-5501
- OpenAlex
- W1977442378
- Cited by
- 254
- References
- 1
- FWCI
- 37.11
- Type
- journal article
- Language
- en
- Open access
- closed
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