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Ultra-thin anatase TiO2nanosheets dominated with {001} facets: thickness-controlled synthesis, growth mechanism and water-splitting properties
Abstract
Ultra-thin anatase TiO2 nanosheets with dominant {001} facets (∼82%) and controllable thickness (1.6–2.7 nm) were synthesized by using a modified one-pot hydrothermal route. As a morphology controlling agent, the concentration of hydrofluoric acid has a significant impact on the thickness of the as-synthesized TiO2 nanosheets. In addition, according to the XRD patterns and TEM images of the products on different reaction stages, the growth process of TiO2 nanosheets was clarified for the first time. We further measured the efficiency for H2 evolution of the ultra-thin anatase TiO2 nanosheets loaded with 1 wt% Pt from photochemical reduction of water in the presence of methanol as a scavenger. The TiO2 nanosheets exhibited a H2 evolution rate as high as 7381 μmol h−1 g−1 under UV-vis light irradiation, attributing to their exposed reactive {001} facets and high crystallinity.
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Cited by
Titanium Dioxide Crystals with Tailored Facets
Liu, G., Yang, H. G., Pan, J., Yang, Y. Q., Lu, G. Q. (., & Cheng, H.-M. (2014) · Chemical Reviews · doi:10.1021/cr400621z · Cited by 1,084
Self-citationOng, W., Tan, L., Chai, S., Yong, S., & Mohamed, A. R. (2014) · ChemSusChem · doi:10.1002/cssc.201300924 · Cited by 339
Li, B., Zhao, Z., Zhou, Q., Meng, B., Meng, X., & Qiu, J. (2014) · Chemistry – A European Journal · doi:10.1002/chem.201402664 · Cited by 95
Metadata
- Authors
- Yang, X. H., Li, Z., Liu, G., Xing, J., Sun, C., Yang, H. G., & Li, C.
- Venue
- CrystEngComm
- Publisher
- Royal Society of Chemistry (RSC)
- Published
- 2011
- Volume
- 13
- Issue
- 5
- Pages
- 1378-1383
- ISSN
- 1466-8033 (ISSN-L)
- OpenAlex
- W2111074923
- Cited by
- 199
- References
- 0
- FWCI
- 6.08
- Type
- journal article
- Language
- en
- Open access
- closed
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- CoChat. (2026). Citation check: Ultra-thin anatase TiO2nanosheets dominated with {001} facets: thickness-controlled synthesis, growth mechanism and water-splitting properties. https://app.cochat.ai/papers/10.1039/c0ce00233j
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- Yang, X. H., Li, Z., Liu, G., Xing, J., Sun, C., Yang, H. G., & Li, C. (2011). Ultra-thin anatase TiO2nanosheets dominated with {001} facets: thickness-controlled synthesis, growth mechanism and water-splitting properties. CrystEngComm. https://doi.org/10.1039/c0ce00233j
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