The DOI matches its Crossref record; 2 of the 2 references it cites were found in a registry or an index.
Direct electro-deposition of graphene from aqueous suspensions
Abstract
We describe the direct electro-chemical reduction of graphene oxide to graphene from aqueous suspension by applying reduction voltages exceeding -1.0 to -1.2 V. The conductivity of the deposition medium is of crucial importance and only values between 4-25 mS cm(-1) result in deposition. Above 25 mS cm(-1) the suspension de-stabilises while conductivities below 4 mS cm(-1) do not show a measurable deposition rate. Furthermore, we show that deposition can be carried out over a wide pH region ranging from 1.5 to 12.5. The electro-deposition process is characterised in terms of electro-chemical methods including cyclic voltammetry, quartz crystal microbalance, impedance spectroscopy, constant amperometry and potentiometric titrations, while the deposits are analysed via Raman spectroscopy, infra-red spectroscopy, X-ray photoelectron spectroscopy and X-ray diffractometry. The determined oxygen contents are similar to those of chemically reduced graphene oxide, and the conductivity of the deposits was found to be ∼20 S cm(-1).
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Citations
Cites
Graphene: Status and Prospects
Geim, A. K. (2009) · Science · doi:10.1126/science.1158877 · Cited by 13,942
Narrow graphene nanoribbons from carbon nanotubes
Jiao, L., Zhang, L., Wang, X., Diankov, G., & Dai, H. (2009) · Nature · doi:10.1038/nature07919 · Cited by 2,441
Metadata
- Authors
- Hilder, M., Winther-Jensen, B., Li, D., Forsyth, M., & MacFarlane, D. R.
- Venue
- Physical Chemistry Chemical Physics
- Publisher
- Royal Society of Chemistry (RSC)
- Published
- 2011
- Volume
- 13
- Issue
- 20
- Pages
- 9187
- ISSN
- 1463-9076 (ISSN-L)
- 1463-9084
- OpenAlex
- W2022482742
- Cited by
- 234
- References
- 2
- FWCI
- 7.75
- Type
- journal article
- Language
- en
- Open access
- closed
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- Hilder, M., Winther-Jensen, B., Li, D., Forsyth, M., & MacFarlane, D. R. (2011). Direct electro-deposition of graphene from aqueous suspensions. Physical Chemistry Chemical Physics. https://doi.org/10.1039/c1cp20173e
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