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One-pot reduction of 5-hydroxymethylfurfural via hydrogen transfer from supercritical methanol
Open accessAbstract
Catalytic conversion of HMF to valuable chemicals was achieved over a Cu-doped porous metal oxide in supercritical methanol. The hydrotalcite catalyst precursor is prepared following simple synthetic procedures, using inexpensive and earth-abundant starting materials in aqueous solutions. The hydrogen equivalents needed for the reductive deoxygenation of HMF originate from the solvent itself upon its reforming. Dimethylfuran, dimethyltetrahydrofuran and 2-hexanol were obtained in good yields. At milder reaction temperatures, a combined yield (DMF + DMTHF) of 58% was achieved. Notably, the formation of higher boiling side products and undesired char from HMF is not detected under these reaction conditions.
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Bozell, J. J., & Petersen, G. R. (2010) · Green Chemistry · doi:10.1039/b922014c · Cited by 4,566
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Barta, K., & Ford, P. C. (2014) · Accounts of Chemical Research · doi:10.1021/ar4002894 · Cited by 373
Self-citationDe, S., Saha, B., & Luque, R. (2015) · Bioresource Technology · doi:10.1016/j.biortech.2014.09.065 · Cited by 359
Gilkey, M. J., Panagiotopoulou, P., Mironenko, A. V., Jenness, G. R., Vlachos, D. G., & Xu, B. (2015) · ACS Catalysis · doi:10.1021/acscatal.5b00586 · Cited by 316
Nilges, P., & Schröder, U. (2013) · Energy & Environmental Science · doi:10.1039/c3ee41857j · Cited by 295
Metadata
- Authors
- Hansen, T. S., Barta, K., Anastas, P. T., Ford, P. C., & Riisager, A.
- Venue
- Green Chemistry
- Publisher
- Royal Society of Chemistry (RSC)
- Published
- 2012
- Volume
- 14
- Issue
- 9
- Pages
- 2457
- ISSN
- 1463-9262 (ISSN-L)
- 1463-9270
- OpenAlex
- W2080794238
- Cited by
- 186
- References
- 1
- FWCI
- 7.67
- Type
- journal article
- Language
- en
- Open access
- green
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- Hansen, T. S., Barta, K., Anastas, P. T., Ford, P. C., & Riisager, A. (2012). One-pot reduction of 5-hydroxymethylfurfural via hydrogen transfer from supercritical methanol. Green Chemistry. https://doi.org/10.1039/c2gc35667h
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Contains information from the Semantic Scholar Academic Graph Datasets, made available under the ODC Attribution License (ODC-BY 1.0).
Semantic Scholar’s data is described in: Kinney, R., et al. (2023). The Semantic Scholar Open Data Platform. arXiv:2301.10140.
