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Efficient hydrogen production and photocatalytic reduction of nitrobenzene over a visible-light-responsive metal–organic framework photocatalyst
Abstract
Efficient hydrogen production and photocatalytic reduction of nitrobenzene were achieved by using a Pt-deposited amino-functionalised Ti(IV) metal–organic framework (Pt/Ti-MOF-NH2) under visible-light irradiation. XRD and N2 adsorption measurements revealed that crystalline microporous structures were formed and maintained even after the Pt deposition. The photocatalytic activity for the visible-light-promoted hydrogen production was improved through the optimization of the deposition amount of Pt as a cocatalyst. The optimised amount of Pt was determined to be 1.5 wt%. The results of in situ ESR measurements clearly indicate that the reaction proceeds through the electron transfer from the organic linker to deposited Pt as a cocatalyst by way of titanium-oxo clusters. In addition, the Pt/Ti-MOF-NH2 photocatalyst was found to catalyse photocatalytic reduction of nitrobenzene under visible-light irradiation. It was also confirmed that the catalyst can be reused at least three times without significant loss of its catalytic activity.
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Cites
Metal-organic framework materials as catalysts
Lee, J., Farha, O. K., Roberts, J., Scheidt, K. A., Nguyen, S. T., & Hupp, J. T. (2009) · Chemical Society Reviews · doi:10.1039/b807080f · Cited by 7,969
Millward, A. R., & Yaghi, O. M. (2005) · Journal of the American Chemical Society · doi:10.1021/ja0570032 · Cited by 2,876
Cited by
Yan, Y., Li, C., Wu, Y., Gao, J., & Zhang, Q. (2020) · Journal of Materials Chemistry A · doi:10.1039/d0ta03749d · Cited by 260
Metadata
- Authors
- Toyao, T., Saito, M., Horiuchi, Y., Mochizuki, K., Iwata, M., Higashimura, H., & Matsuoka, M.
- Venue
- Catalysis Science & Technology
- Publisher
- Royal Society of Chemistry (RSC)
- Published
- 2013
- Volume
- 3
- Issue
- 8
- Pages
- 2092
- ISSN
- 2044-4753 (ISSN-L)
- 2044-4761
- OpenAlex
- W1993274077
- Cited by
- 220
- References
- 2
- FWCI
- 9.58
- Type
- journal article
- Language
- en
- Open access
- closed
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- Toyao, T., Saito, M., Horiuchi, Y., Mochizuki, K., Iwata, M., Higashimura, H., & Matsuoka, M. (2013). Efficient hydrogen production and photocatalytic reduction of nitrobenzene over a visible-light-responsive metal–organic framework photocatalyst. Catalysis Science & Technology. https://doi.org/10.1039/c3cy00211j
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Semantic Scholar’s data is described in: Kinney, R., et al. (2023). The Semantic Scholar Open Data Platform. arXiv:2301.10140.
