The DOI matches its Crossref record; 1 of the 1 references it cites were found in a registry or an index.
Size- and morphology-controlled NH2-MIL-53(Al) prepared in DMF–water mixed solvents
Abstract
We present here a simple solvothermal method to fabricate metal-organic framework NH2-MIL-53(Al) crystals with controllable size and morphology just by altering the ratio of water in the DMF-water mixed solvent system without the addition of any surfactants or capping agents. With increasing the volume ratio of water in the mixed solvents, a series of NH2-MIL-53(Al) crystals with different sizes and morphologies were synthesized. The average size of the smallest crystal is 76 ± 20 nm, which provides us a simple and environmentally friendly way to prepare nanoscale MOFs. The largest BET surface area of these samples is 1882 m(2) g(-1) that is mainly contributed by its micropore surface area, and its corresponding micropore volume is 0.83 cm(3) g(-1), which have greatly extended its application in the fields of gas adsorption and postsynthetic modification. All these samples were characterized by SEM, XRD, N2 adsorption/desorption, TGA and FT-IR. Then a mechanism for the impact of the water ratio on the crystal size and morphology is presented and discussed.
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Cites
BioMOFs: Metal–Organic Frameworks for Biological and Medical Applications
McKinlay, A. C., Morris, R. E., Horcajada, P., Férey, G., Gref, R., Couvreur, P., & Serre, C. (2010) · Angewandte Chemie International Edition · doi:10.1002/anie.201000048 · Cited by 1,256
Cited by
Nanoscale covalent organic frameworks: from controlled synthesis to cancer therapy
He, X., Jiang, Z., Akakuru, O. U., Li, J., & Wu, A. (2021) · Chemical Communications · doi:10.1039/d1cc04846e · Cited by 303
Solvothermal synthesis of NH2-MIL-125(Ti) from circular plate to octahedron
Hu, S., Liu, M., Li, K., Zuo, Y., Zhang, A., Song, C., Zhang, G., & Guo, X. (2014) · CrystEngComm · doi:10.1039/c4ce01545b · Cited by 269
Self-citationAbdi, J., Sisi, A. J., Hadipoor, M., & Khataee, A. (2022) · Journal of Hazardous Materials · doi:10.1016/j.jhazmat.2021.127558 · Cited by 144
M., P., Asha, K. S., Sinha, M., Poduval, A., & Mandal, S. (2016) · CrystEngComm · doi:10.1039/c5ce01886b · Cited by 24
Metadata
- Authors
- Cheng, X., Zhang, A., Hou, K., Liu, M., Wang, Y., Song, C., Zhang, G., & Guo, X.
- Venue
- Dalton Transactions
- Publisher
- Royal Society of Chemistry (RSC)
- Published
- 2013
- Volume
- 42
- Issue
- 37
- Pages
- 13698
- ISSN
- 1477-9226 (ISSN-L)
- 1477-9234
- OpenAlex
- W2168788420
- Cited by
- 308
- References
- 1
- FWCI
- 5.50
- Type
- journal article
- Language
- en
- Open access
- closed
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- Cheng, X., Zhang, A., Hou, K., Liu, M., Wang, Y., Song, C., Zhang, G., & Guo, X. (2013). Size- and morphology-controlled NH2-MIL-53(Al) prepared in DMF–water mixed solvents. Dalton Transactions. https://doi.org/10.1039/c3dt51322j
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