The DOI matches its Crossref record; 6 of the 6 references it cites were found in a registry or an index.
Facile extraction of thermally stable cellulose nanocrystals with a high yield of 93% through hydrochloric acid hydrolysis under hydrothermal conditions
Abstract
A facile approach for extracting cellulose nanocrystals (CNCs) was presented through hydrochloric acid hydrolysis of cellulose raw materials under hydrothermal conditions. The influences of preparation parameters, such as reaction time, reaction temperature, and acid-to-cellulose raw material ratio, and different neutralization methods on the yield, microstructure and properties were studied. A high yield of up to 93.7%, crystallinity of 88.6%, and a maximum degradation temperature (Tmax) of 363.9 °C can be achieved by combining hydrochloric acid hydrolysis under hydrothermal conditions and neutralization with ammonia, compared with only 30.2%, 84.3% and 253.2 °C for sulfuric acid hydrolysis, respectively. More importantly, good stability of aqueous CNC suspensions can also be obtained due to the existence of ammonium groups, which can easily be removed through simple heat treatment before using the CNCs.
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Cites
Cellulose nanocrystals: chemistry, self-assembly, and applications
Habibi, Y., Lucia, L. A., & Rojas, O. J. (2010) · Chemical Reviews · doi:10.1021/cr900339w · Cited by 5,980
Optimization of the isolation of nanocrystals from microcrystalline cellulose by acid hydrolysis
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Bacterial cellulose nanocrystals exhibiting high thermal stability and their polymer nanocomposites
George, J., Ramana, K. V., Bawa, A. S., & Siddaramaiah (2011) · International Journal of Biological Macromolecules · doi:10.1016/j.ijbiomac.2010.09.013 · Cited by 319
Permselective nanostructured membranes based on cellulose nanowhiskers
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Cited by
Wood-Derived Materials for Green Electronics, Biological Devices, and Energy Applications
Zhu, H., Luo, W., Ciesielski, P. N., Fang, Z., Zhu, J. Y., Henriksson, G., Himmel, M. E., & Hu, L. (2016) · Chemical Reviews · doi:10.1021/acs.chemrev.6b00225 · Cited by 1,532
Nanocellulose-based foams and aerogels: processing, properties, and applications
Lavoine, N., & Bergström, L. (2017) · Journal of Materials Chemistry A · doi:10.1039/c7ta02807e · Cited by 656
Wood-based nanotechnologies toward sustainability
Jiang, F., Li, T., Li, Y., Zhang, Y., Gong, A., Dai, J., Hitz, E., Luo, W., & Hu, L. (2018) · Advanced Materials · doi:10.1002/adma.201703453 · Cited by 599
Advances in cellulose nanomaterials
Kargarzadeh, H., Mariano, M., Gopakumar, D., Ahmad, I., Thomas, S., Dufresne, A., Huang, J., & Lin, N. (2018) · Cellulose · doi:10.1007/s10570-018-1723-5 · Cited by 508
Use of nanocellulose in printed electronics: a review
Hoeng, F., Denneulin, A., & Bras, J. (2016) · Nanoscale · doi:10.1039/c6nr03054h · Cited by 459
Metadata
- Authors
- Yu, H., Qin, Z., Liang, B., Liu, N., Zhou, Z., & Chen, L.
- Venue
- Journal of Materials Chemistry A
- Publisher
- Royal Society of Chemistry (RSC)
- Published
- 2013
- Volume
- 1
- Issue
- 12
- Pages
- 3938
- ISSN
- 2050-7488 (ISSN-L)
- 2050-7496
- OpenAlex
- W2029330110
- Cited by
- 518
- References
- 6
- FWCI
- 7.31
- Type
- journal article
- Language
- en
- Open access
- closed
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- Yu, H., Qin, Z., Liang, B., Liu, N., Zhou, Z., & Chen, L. (2013). Facile extraction of thermally stable cellulose nanocrystals with a high yield of 93% through hydrochloric acid hydrolysis under hydrothermal conditions. Journal of Materials Chemistry A. https://doi.org/10.1039/c3ta01150j
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Contains information from the Semantic Scholar Academic Graph Datasets, made available under the ODC Attribution License (ODC-BY 1.0).
Semantic Scholar’s data is described in: Kinney, R., et al. (2023). The Semantic Scholar Open Data Platform. arXiv:2301.10140.
