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Pd/C as a Highly Active Catalyst for Heck, Suzuki and Sonogashira Reactions
Abstract
A specially optimized air-stable Pd on activated carbon catalyst is demonstrated to be a highly active (TON up to 36,000), selective and convenient heterogeneous catalyst for CC couplings of aryl halides in Heck, Suzuki, and Sonogashira reactions. The Pd/C catalyst developed allows extremely low Pd concentrations (down to 0.0025 mol% for Heck coupling, 0.005 mol% for Suzuki coupling) and high conversions of aryl bromides within a few hours. Easy and complete Pd separation and recovery is possible.
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Citations
Cited by
Carbon−Carbon Coupling Reactions Catalyzed by Heterogeneous Palladium Catalysts
Yin, & Liebscher, J. (2007) · Chemical Reviews · doi:10.1021/cr0505674 · Cited by 2,085
Phan, N. T. S., Van Der Sluys, M., & Jones, C. W. (2006) · Advanced Synthesis & Catalysis · doi:10.1002/adsc.200505473 · Cited by 1,905
Scheuermann, G. M., Rumi, L., Steurer, P., Bannwarth, W., & Mülhaupt, R. (2009) · Journal of the American Chemical Society · doi:10.1021/ja901105a · Cited by 1,163
Asymmetric Catalysis at Chiral Metal Surfaces
Mallat, T., Orglmeister, E., & Baiker, A. (2007) · Chemical Reviews · doi:10.1021/cr0683663 · Cited by 592
Alonso, F., Beletskaya, I. P., & Yus, M. (2005) · Tetrahedron · doi:10.1016/j.tet.2005.08.054 · Cited by 498
Metadata
- Authors
- Heidenreich, R. G., Köhler, K., Krauter, J. G. E., & Pietsch, J.
- Venue
- Synlett
- Publisher
- Georg Thieme Verlag KG
- Published
- 2002
- Volume
- 2002
- Issue
- 07
- Pages
- 1118-1122
- ISSN
- 0936-5214 (ISSN-L)
- 1437-2096
- OpenAlex
- W2949725387
- Cited by
- 200
- References
- 0
- FWCI
- 14.42
- Type
- journal article
- Language
- en
- Open access
- closed
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- Heidenreich, R. G., Köhler, K., Krauter, J. G. E., & Pietsch, J. (2002). Pd/C as a Highly Active Catalyst for Heck, Suzuki and Sonogashira Reactions. Synlett. https://doi.org/10.1055/s-2002-32589
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Semantic Scholar’s data is described in: Kinney, R., et al. (2023). The Semantic Scholar Open Data Platform. arXiv:2301.10140.
