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The density of supercooled water. II. Bulk samples cooled to the homogeneous nucleation limit
Abstract
We have measured the density of supercooled water (H2O) in the range −33.41≤T≤−5.23 °C. Our samples were held in glass capillary tubing with an approximate inside diameter of 0.3 mm=300 μ. These samples were prepared by Mossop’s method and could be cooled to their homogeneous nucleation limit before freezing. We compare our density data to other measurements using capillaries and demonstrate what appears to be an excess density in smaller capillaries which is inversely proportional to the capillary inside diameter. The origins of this excess density are unknown, but we show its effect is insignificant on our measurement. The thermal expansivities derived from our data are fit to a power law in temperature relative to a singular temperature. These results are inconclusive due to a poor knowledge of the background expansivity.
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Cited by
Homogeneous Ice Nucleation at Moderate Supercooling from Molecular Simulation
Sanz, E., Vega, C., Espinosa, J. R., Caballero-Bernal, R., Abascal, J. L. F., & Valeriani, C. (2013) · Journal of the American Chemical Society · doi:10.1021/ja4028814 · Cited by 334
Shi, G., Liu, G., Su, C., Chen, H., Chen, Y., Su, Y., Müller, A. J., & Wang, D. (2017) · Macromolecules · doi:10.1021/acs.macromol.7b02284 · Cited by 50
Metadata
- Authors
- Hare, D. E., & Sorensen, C. M.
- Venue
- The Journal of Chemical Physics
- Publisher
- AIP Publishing
- Published
- 1987-10-15
- Volume
- 87
- Issue
- 8
- Pages
- 4840-4845
- ISSN
- 0021-9606 (ISSN-L)
- 1089-7690
- OpenAlex
- W1977851577
- Cited by
- 238
- References
- 0
- FWCI
- 0.46
- Type
- journal article
- Language
- en
- Open access
- closed
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- CoChat. (2026). Citation check: The density of supercooled water. II. Bulk samples cooled to the homogeneous nucleation limit. https://app.cochat.ai/papers/10.1063/1.453710
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- Hare, D. E., & Sorensen, C. M. (1987). The density of supercooled water. II. Bulk samples cooled to the homogeneous nucleation limit. The Journal of Chemical Physics. https://doi.org/10.1063/1.453710
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