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Single-crystal X-ray diffraction at megabar pressures and temperatures of thousands of degrees
Open accessAbstract
The most reliable information about crystal structures and their response to changes in pressure and temperature is obtained from single-crystal diffraction experiments. We have developed a methodology to perform single-crystal X-ray diffraction experiments in laser-heated diamond anvil cells and demonstrate that structural refinements and accurate measurements of the thermal equation of state of metals, oxides and silicates from single-crystal intensity data are possible in pressures ranging up to megabars and temperatures of thousands of degrees. A new methodology was applied to solve the in situ high pressure, high temperature structure of iron oxide and study structural variations of iron and aluminum bearing silicate perovskite at conditions of the Earth's lower mantle.
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“In the last 15 years, an upgrade in synchrotron diffraction protocols for single crystal diffraction at extreme conditions has allowed experimental ab-initio determination of structures after multiple phase transitions (Dera et al., 2005;Dubrovinsky et al., 2010;Merlini & Hanfland, 2013).”
From Structures and Crystal Chemistry of Carbonate at Earth's Mantle Conditions (2020) · cites this paper as Dubrovinsky et al., 2010
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Structures and Crystal Chemistry of Carbonate at Earth's Mantle Conditions
Merlini, M., Milani, S., & Maurice, J. (2020) · Geophysical Monograph Series · doi:10.1002/9781119508229.ch9 · Cited by 7
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Metadata
- Authors
- Dubrovinsky, L., Boffa-Ballaran, T., Glazyrin, K., Kurnosov, A., Frost, D., Merlini, M., Hanfland, M., Prakapenka, V. B., Schouwink, P., Pippinger, T., & Dubrovinskaia, N.
- Affiliations
- University of Bayreuth (DE)
- University of Milan (IT)
- European Synchrotron Radiation Facility (FR)
- University of Chicago (US)
- Heidelberg University (DE)
- Corresponding author
- Dubrovinsky, L.
- ORCID
- Venue
- High Pressure Research
- Publisher
- Informa UK Limited
- Published
- 2010-12
- Volume
- 30
- Issue
- 4
- Pages
- 620-633
- ISSN
- 0895-7959 (ISSN-L)
- 1477-2299
- OpenAlex
- W2014713350
- Cited by
- 68
- References
- 0
- Citations by year
- 2024: 1 · 2023: 4 · 2021: 2 · 2020: 8 · 2019: 3 · 2018: 6 · 2017: 1 · 2016: 6 · 2015: 7 · 2014: 4 · 2013: 15 · 2012: 9
- FWCI
- 7.27
- Type
- journal article
- Language
- en
- Open access
- bronze
- doi.org
- Locations
- High Pressure Research (publishedVersion)
- ERef Bayreuth (University of Bayreuth) (submittedVersion)
- Archivio Istituzionale della Ricerca (Universita Degli Studi Di Milano) (submittedVersion, other-oa)
- Funders
- Deutsche Forschungsgemeinschaft
- European Synchrotron Radiation Facility
- Topics
- Physical Sciences › Earth and Planetary Sciences › Geophysics › High-pressure geophysics and materials
- Physical Sciences › Materials Science › Materials Chemistry › X-ray Diffraction in Crystallography
- Physical Sciences › Materials Science › Materials Chemistry › Boron and Carbon Nanomaterials Research
- Keywords
- single-crystal X-ray diffraction, megabar pressure, high-temperature crystal structure, laser-heated diamond anvil cell, thermal equation of state, iron oxide, silicate perovskite, lower mantle, structure refinement
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