The DOI matches its Crossref record; 7 of the 7 references it cites were found in a registry or an index.
Nuclear-Magnetic-Resonance Line Narrowing by a Rotating rf Field
Abstract
A nuclear-magnetic-resonance method is explored, which effectively attenuates the dipolar interaction in solids. The experimental technique corresponds to the observation of a free-induction decay in a frame of reference rotating with the frequency of an applied rf field. When the amplitude ${H}_{1}$ of this field is much greater than the local field in the solid, and when its frequency is appropriately chosen, the secular part of the dipolar interaction is removed. As a result the rotary saturation line is extremely narrowed. At smaller values of ${H}_{1}$, nonsecular terms in the dipolar interaction come into play and contribute to line broadening. These nonsecular effects are investigated both theoretically and experimentally. All the measurements were made in single crystals of calcium fluoride. The calculation of the nonsecular contribution to the line width utilizes the unitary transformation method of Jordhal and Pryce. Theory and experiment are in good agreement.
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Cites
The Principles of Nuclear Magnetism
Abragam, A., & Hebel, L. C. (1961) · American Journal of Physics · doi:10.1119/1.1937646 · Cited by 15,792
The Dipolar Broadening of Magnetic Resonance Lines in Crystals
Vleck, J. H. V. (1948) · Physical Review · doi:10.1103/physrev.74.1168 · Cited by 2,835
Principles of Magnetic Resonance
Slichter, C. P. (1978) · Springer Series in Solid-State Sciences · doi:10.1007/978-3-662-12784-1 · Cited by 1,876
Nuclear Magnetic Resonance Spectra from a Crystal rotated at High Speed
ANDREW, E. R., BRADBURY, A., & EADES, R. G. (1958) · Nature · doi:10.1038/1821659a0 · Cited by 1,255
Free Induction Decays of Rotating Solids
Lowe, I. J. (1959) · Physical Review Letters · doi:10.1103/physrevlett.2.285 · Cited by 1,170
Nuclear Magnetic Resonance Saturation and Rotary Saturation in Solids
Redfield, A. G. (1955) · Physical Review · doi:10.1103/physrev.98.1787 · Cited by 888
Removal of Dipolar Broadening of Nuclear Magnetic Resonance Spectra of Solids by Specimen Rotation
ANDREW, E. R., BRADBURY, A., & EADES, R. G. (1959) · Nature · doi:10.1038/1831802a0 · Cited by 714
Cited by
Coherent Averaging Effects in Magnetic Resonance
Haeberlen, U., & Waugh, J. S. (1968) · Physical Review · doi:10.1103/physrev.175.453 · Cited by 1,083
Frequency-switched pulse sequences: Homonuclear decoupling and dilute spin NMR in solids
Bielecki, A., Kolbert, A. C., & Levitt, M. H. (1989) · Chemical Physics Letters · doi:10.1016/0009-2614(89)87166-0 · Cited by 485
Nanochannels of Two Distinct Cross-Sections in a Porous Al-Based Coordination Polymer
Comotti, A., Bracco, S., Sozzani, P., Horike, S., Matsuda, R., Chen, J., Takata, M., Kubota, Y., & Kitagawa, S. (2008) · Journal of the American Chemical Society · doi:10.1021/ja802589u · Cited by 302
Li, S., & Hong, M. (2011) · Journal of the American Chemical Society · doi:10.1021/ja108943n · Cited by 296
Investigation of Molecular Motions by Lee-Goldburg Cross-Polarization NMR Spectroscopy
Hong, M., Yao, X., Jakes, K., & Huster, D. (2002) · The Journal of Physical Chemistry B · doi:10.1021/jp0156064 · Cited by 137
Metadata
- Authors
- Lee, M., & Goldburg, W. I.
- Venue
- Physical Review
- Publisher
- American Physical Society (APS)
- Published
- 1965-11-15
- Volume
- 140
- Issue
- 4A
- Pages
- A1261-A1271
- ISSN
- 0031-899X (ISSN-L)
- OpenAlex
- W2029561831
- Cited by
- 656
- References
- 7
- FWCI
- 3.83
- Type
- journal article
- Language
- en
- Open access
- closed
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Bibliographic data: Semantic Scholar, OpenAlex, Crossref.
Contains information from the Semantic Scholar Academic Graph Datasets, made available under the ODC Attribution License (ODC-BY 1.0).
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