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Structure Determination of the Two-Domain (1×4) AnataseTiO2(001)Surface
Abstract
The reconstructed anatase ${\mathrm{TiO}}_{2}(001)$ surface has been investigated by low-energy electron diffraction (LEED), x-ray photoelectron spectroscopy (XPS), and angle-resolved mass spectroscopy of recoiled ions (AR-MSRI). Prior investigations have observed or considered only a $(1\ifmmode\times\else\texttimes\fi{}1)$ unreconstructed termination for this surface with no detailed structural analysis. Our LEED results indicate a previously unobserved two-domain $(1\ifmmode\times\else\texttimes\fi{}4)$ reconstruction after sputtering and annealing the $(1\ifmmode\times\else\texttimes\fi{}1)$ surface. The XPS data for this reconstruction indicate the presence of only ${\mathrm{Ti}}^{4+}$. Simulations of the AR-MSRI experimental data indicate a best fit for a microfaceted surface, revealing both (103) and $(\overline{1}03)$ surface planes.
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Cites
Photocatalysis on TiO2 Surfaces: Principles, Mechanisms, and Selected Results
Linsebigler, A. L., Lu, G., & Yates, J. T. (1995) · Chemical Reviews · doi:10.1021/cr00035a013 · Cited by 11,575
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The surface science of titanium dioxide
Diebold, U. (2003) · Surface Science Reports · doi:10.1016/s0167-5729(02)00100-0 · Cited by 7,944
Why is anatase a better photocatalyst than rutile? - Model studies on epitaxial TiO2 films
Luttrell, T., Halpegamage, S., Tao, J., Kramer, A., Sutter, E., & Batzill, M. (2014) · Scientific Reports · doi:10.1038/srep04043 · Cited by 1,544
Structure and energetics of stoichiometricTiO2anatase surfaces
Lazzeri, M., Vittadini, A., & Selloni, A. (2001) · Physical Review B · doi:10.1103/physrevb.63.155409 · Cited by 1,454
Facet Effect of Single-Crystalline Ag3PO4 Sub-microcrystals on Photocatalytic Properties
Bi, Y., Ouyang, S., Umezawa, N., Cao, J., & Ye, J. (2011) · Journal of the American Chemical Society · doi:10.1021/ja2002132 · Cited by 1,316
Metadata
- Authors
- Herman, G. S., Sievers, M. R., & Gao, Y.
- Venue
- Physical Review Letters
- Publisher
- American Physical Society (APS)
- Published
- 2000-04-10
- Volume
- 84
- Issue
- 15
- Pages
- 3354-3357
- ISSN
- 0031-9007 (ISSN-L)
- 1079-7114
- OpenAlex
- W1983453717
- Cited by
- 211
- References
- 1
- FWCI
- 6.40
- Type
- journal article
- Language
- en
- Open access
- closed
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- Herman, G. S., Sievers, M. R., & Gao, Y. (2000). Structure Determination of the Two-Domain (1×4) AnataseTiO2(001)Surface. Physical Review Letters. https://doi.org/10.1103/physrevlett.84.3354
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