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Binder Distribution in Ceramic Greenware During Thermolysis
Abstract
Capillary forces were shown to influence the distribution of polymer‐plasicizer mixtures within ceramic green bodies during binder thermolysis. Isothermal thermogravimetric analysis was performed on tape‐cast sheets of an aluminapoly(vinyl butyrall‐dibutyl phthalate composite and direct observations were made of the binder distribution and pore growth after partial pyrolysis. This led to the investigation of a model system, an alumina‐eicosane composite, by similar experimental techniques. The early stage of binder removal was found to be similar to the drying of particle beds in which capillary forces draw liquid into the smaller pores at the surface. The morphology of the binder distribution produced by these processes dictates which mass‐transfer resistances may be controlling in binder burnout. A model is described that determines the length scale over which capillarity acts based on measurable physical parameters of the binder system and the packing of the ceramic particles.
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References 12 · Cited by 151
Research works printed but not linked: 11
- Mistler R. E., 1978, Ceramic Processing Before Firing, 411
- 10.1016/0021-9797(81)90132-6 · DOI
- Pearse J. F., 1949, The Mechanism of the Drying of Solids, Trans. Inst. Chem. Eng., 27, 1
- 10.1021/ie50298a017 · DOI
- Ceaglske N. H., 1937, The Drying of Granular Solids, Trans. Am. Inst. Chem. Eng., 33, 283
- 10.1111/j.1151-2916.1986.tb04688.x · DOI
- 10.1111/j.1151-2916.1989.tb06280.x · DOI
- 10.1017/S0021859600018499 · DOI
- Collins R. E., 1961, Flow of Fluids Through Porous Materials, 54
- Geffen T. M., 1951, Experimental Investigation of Factors Affecting Laboratory Relative Permeability Measurements., Petroleum Trans., AIME, 192, 99
- B. C.Mutsuddy.A Review of Binder Removal Processes for Ceramic Injection Molded Parts ”AIChE Conference on Emerging Technologies in Materials Minneapolis MN Aug. 1820 1987.
Metadata
- Authors
- Cima, M. J., Lewis, J. A., & Devoe, A. D.
- Affiliations
- American Ceramic Society (US)
- Massachusetts Institute of Technology (US)
- Venue
- Journal of the American Ceramic Society
- Publisher
- Wiley
- Published
- 1989-07
- Volume
- 72
- Issue
- 7
- Pages
- 1192-1199
- ISSN
- 0002-7820 (ISSN-L)
- 1551-2916
- OpenAlex
- W2103284055
- Cited by
- 151
- References
- 12
- Citations by year
- 2026: 7 · 2025: 3 · 2024: 2 · 2023: 3 · 2022: 2 · 2021: 2 · 2020: 4 · 2019: 1 · 2018: 3 · 2017: 2 · 2016: 1 · 2015: 3 · 2014: 3 · 2013: 3 · 2012: 2
- FWCI
- 10.37
- Type
- journal article
- Language
- en
- Open access
- closed
- Locations
- Journal of the American Ceramic Society (publishedVersion)
- Topics
- Physical Sciences › Materials Science › Ceramics and Composites › Advanced ceramic materials synthesis
- Physical Sciences › Engineering › Industrial and Manufacturing Engineering › Additive Manufacturing and 3D Printing Technologies
- Physical Sciences › Materials Science › Materials Chemistry › Thermal and Kinetic Analysis
- Keywords
- binder distribution, ceramic green bodies, capillary forces, polyvinyl butyral, dibutyl phthalate, alumina, eicosane, binder burnout, mass transfer resistance, pore growth, particle packing
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