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Functional characterization of bimetallic CuPd x nanoparticles in hydrothermal conversion of glycerol to lactic acid
Abstract
The crude glycerol from biomass represents an abundant and inexpensive resource which can be utilized in producing food additives such as lactic acid. The direct transformation of bioderived glycerol to lactic acid under the catalysis of bimetallic CuPd x nanoparticles as well as monometallic Cu and Pd was investigated in hydrothermal conditions. The properties of fresh and spent bimetallic CuPd x nanoparticles were characterized with various physicochemical techniques viz. XRD, TEM, HRTEM, XPS, and AAS measurements. Catalytic activity of the prepared CuPd x nanoparticles is superior to the monometallic ones due to the alloying trend and synergistic effects. At optimal experimental conditions (100 ml of glycerol and NaOH solution, catalyst/glycerol mass ratio 2:100, 220°C, and 2.0 hr), the desired lactic acid selectivity catalyzed by the bimetallic CuPd 2 , CuPd 3 , and CuPd 4 catalysts reached 95.3%, 91.4%, and 90.9%, respectively. PRACTICAL APPLICATIONS: Lactic acid, a widely used food additive, was traditionally produced by fermentation. However, due to the limitation such as time-consuming and complex separation procedure, interest has been attracted in developing an alternative approach toward efficient production of lactic acid. An attempt was made in present study to use the biodiesel byproduct, glycerol, and chemical conversion to high-valued lactic acid. Compared with traditional biological fermentation route, it was evidenced that glycerol selective transformation t…
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“Although extensive research has shown that noble metal-based materials generally exhibit the highest HER activity, their limited natural abundance and prohibitive costs severely restrict their widespread commercialization [9–13].”
From Rational synthesis of Au3Cu@Rhx core–shell aerogel electrocatalysts for efficient hydrogen evolution reaction (2026) · cites this paper as [12]
In the citing paper
“Although extensive research has shown that noble metal-based materials generally exhibit the highest HER activity, their limited natural abundance and prohibitive costs severely restrict their widespread commercialization [9–13].”
From Rational synthesis of Au3Cu@Rhx core–shell aerogel electrocatalysts for efficient hydrogen evolution reaction (2026) · cites this paper as [12]
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Metadata
- Authors
- Shen, L., Zhou, X., Zhang, C., Yin, H., Wang, A., & Wang, C.
- Affiliations
- Jiangsu University (CN)
- Beijing Technology and Business University (CN)
- Corresponding author
- Yin, Hengbo
- Wang, Chengtao
- Venue
- Journal of Food Biochemistry
- Publisher
- Wiley
- Published
- 2019-05-29
- Volume
- 43
- Issue
- 8
- Pages
- e12931-e12931
- ISSN
- 0145-8884 (ISSN-L)
- 1745-4514
- OpenAlex
- W2947205226
- Cited by
- 77
- References
- 28
- Citations by year
- 2026: 17 · 2025: 45 · 2024: 6 · 2023: 2 · 2022: 3 · 2021: 1 · 2020: 3
- FWCI
- 0.62
- Type
- journal article
- Language
- en
- Open access
- closed
- Licence
- onlinelibrary.wiley.com/termsAndConditions#vor (vor)
- doi.wiley.com/10.1002/tdm_license_1.1 (tdm)
- Locations
- Journal of Food Biochemistry (publishedVersion)
- PubMed (publishedVersion)
- Funders
- National Natural Science Foundation of China (21506082)
- Topics
- Physical Sciences › Chemical Engineering › Catalysis › Catalysis for Biomass Conversion
- Physical Sciences › Chemical Engineering › Process Chemistry and Technology › Carbon dioxide utilization in catalysis
- Physical Sciences › Chemical Engineering › Process Chemistry and Technology › Subcritical and Supercritical Water Processes
- Keywords
- crude glycerol, lactic acid production, hydrothermal conversion, biodiesel by-product valorization, synergistic catalysis, food additive production, bio-based chemicals
- MeSH terms
- Copper, Glycerol, Palladium, Lactic Acid, Microscopy, Electron, Transmission, Metal Nanoparticles
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