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Synthesis of Imido Analogs of the Uranyl Ion
Abstract
Here we describe the synthesis of two imido analogs of the uranyl ion, UO 2+ 2 , in which the oxygens are replaced by divalent alkyl or aryl nitrogen groups: U(N t Bu) 2 I 2 (THF) 2 (1) and U(NPh) 2 I 2 (THF) 3 (2) (where t Bu is tert -butyl and THF is tetrahydrofuran). Both compounds have been fully characterized by standard analytical techniques, including x-ray crystallography, and the chemical bonding between the metal center and the nitrogen ligands was quantified by using hybrid density functional theory calculations. As expected for a uranyl analog, these complexes exhibit linear N-U-N linkages and very short U-N bonds. In addition, the theoretical calculations show strong involvement of the 5f and 6d electrons in the U-N bonding.
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(1999) · Choice Reviews Online · doi:10.5860/choice.37-0940 · Cited by 14,314
Cited by
Fox, A. R., Bart, S. C., Meyer, K., & Cummins, C. C. (2008) · Nature · doi:10.1038/nature07372 · Cited by 451
Recent Developments in Synthesis and Structural Chemistry of Nonaqueous Actinide Complexes
Jones, M. B., & Gaunt, A. J. (2013) · Chemical Reviews · doi:10.1021/cr300198m · Cited by 323
The vitality of uranium molecular chemistry at the dawn of the XXIst century
Ephritikhine, M. (2006) · Dalton Transactions · doi:10.1039/b603463b · Cited by 314
Metadata
- Authors
- Hayton, T. W., Boncella, J. M., Scott, B. L., Palmer, P. D., Batista, E. R., & Hay, P. J.
- Venue
- Science
- Published
- 2005-12-23
- Volume
- 310
- Issue
- 5756
- Pages
- 1941-1943
- ISSN
- 0036-8075 (ISSN-L)
- 1095-9203
- OpenAlex
- W2083518550
- Cited by
- 232
- References
- 1
- FWCI
- 5.56
- Type
- journal article
- Language
- en
- Open access
- closed
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- Hayton, T. W., Boncella, J. M., Scott, B. L., Palmer, P. D., Batista, E. R., & Hay, P. J. (2005). Synthesis of Imido Analogs of the Uranyl Ion. Science. https://doi.org/10.1126/science.1120069
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