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Electrogeneration of Hydroxyl Radicals on Boron-Doped Diamond Electrodes
Open accessAbstract
The electrogeneration of hydroxyl radicals was studied at a synthetic boron-doped diamond (BDD) thin film electrode. Spin trapping was used for detection of hydroxyl radicals with 5,5-dimethyl-1-pyrroline- N -oxide and with salicylic acid using electron spin resonance and liquid chromatography measurements, respectively. The production of hydrogen peroxide and competitive oxidation of formic and oxalic acids were also investigated using bulk electrolysis. The results have shown that oxidation of salicylic acid leads to the production of hydroxylated products (2,3- and 2,5-dihydroxybenzoic acids). These results demonstrate that the oxidation process on BDD electrodes involves hydroxyl radicals as electrogenerated intermediates. © 2003 The Electrochemical Society. All rights reserved.
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Buxton, G. V., Greenstock, C. L., Helman, W. P., & Ross, A. B. (1988) · Journal of Physical and Chemical Reference Data · doi:10.1063/1.555805 · Cited by 12,332
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Metadata
- Authors
- Marselli, B., Garcia-Gomez, J., Michaud, P.-A., Rodrigo, M. A., & Comninellis, C.
- Venue
- Journal of The Electrochemical Society
- Publisher
- The Electrochemical Society
- Published
- 2003
- Volume
- 150
- Issue
- 3
- Pages
- D79
- ISSN
- 0013-4651 (ISSN-L)
- OpenAlex
- W2160659516
- Cited by
- 969
- References
- 1
- FWCI
- 26.79
- Type
- journal article
- Language
- en
- Open access
- bronze
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- Marselli, B., Garcia-Gomez, J., Michaud, P.-A., Rodrigo, M. A., & Comninellis, C. (2003). Electrogeneration of Hydroxyl Radicals on Boron-Doped Diamond Electrodes. Journal of The Electrochemical Society. https://doi.org/10.1149/1.1553790
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Contains information from the Semantic Scholar Academic Graph Datasets, made available under the ODC Attribution License (ODC-BY 1.0).
Semantic Scholar’s data is described in: Kinney, R., et al. (2023). The Semantic Scholar Open Data Platform. arXiv:2301.10140.
