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Initiation and Growth of Self-Organized TiO[sub 2] Nanotubes Anodically Formed in NH[sub 4]F∕(NH[sub 4])[sub 2]SO[sub 4] Electrolytes
Open accessAbstract
The anodic formation of self-organized porous on titanium was investigated in 1 M electrolytes containing 0.5 wt % by potential sweeps to . By a combination of electrochemical, morphological, and compositional information we show that the sweep rate has a significant influence on the initiation and growth of the porous structures. In the first phase of the anodization process, a precursor barrier type of oxide film is formed; underneath this film pores then start growing first randomly and then self-organize. High-aspect-ratio nanostructures can be obtained under optimized electrochemical conditions. These nanotubular oxide layers have single-pore diameter ranging from 90 to 110 nm, average spacing of 150 nm, and porosity in the order of 37–42%. The current work indicates that the nature of the initial barrier-type layer has a strong influence on establishing optimized pore growth conditions.
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Cites
A low-cost, high-efficiency solar cell based on dye-sensitized colloidal TiO2 films
O'Regan, B., & Grätzel, M. (1991) · Nature · doi:10.1038/353737a0 · Cited by 28,599
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Bamboo-Type TiO2 Nanotubes: Improved Conversion Efficiency in Dye-Sensitized Solar Cells
Kim, D., Ghicov, A., Albu, S. P., & Schmuki, P. (2008) · Journal of the American Chemical Society · doi:10.1021/ja805201v · Cited by 317
Self-citationN-Doping of anodic TiO2 nanotubes using heat treatment in ammonia
Vitiello, R. P., Macak, J. M., Ghicov, A., Tsuchiya, H., Dick, L. F. P., & Schmuki, P. (2006) · Electrochemistry Communications · doi:10.1016/j.elecom.2006.01.023 · Cited by 256
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Metadata
- Authors
- Taveira, L. V., Macák, J. M., Tsuchiya, H., Dick, L. F. P., & Schmuki, P.
- Venue
- Journal of The Electrochemical Society
- Publisher
- The Electrochemical Society
- Published
- 2005
- Volume
- 152
- Issue
- 10
- Pages
- B405
- ISSN
- 0013-4651 (ISSN-L)
- OpenAlex
- W1488595613
- Cited by
- 304
- References
- 1
- FWCI
- 12.50
- Type
- journal article
- Language
- en
- Open access
- bronze
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- CoChat. (2026). Citation check: Initiation and Growth of Self-Organized TiO[sub 2] Nanotubes Anodically Formed in NH[sub 4]F∕(NH[sub 4])[sub 2]SO[sub 4] Electrolytes. https://app.cochat.ai/papers/10.1149/1.2008980
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- Taveira, L. V., Macák, J. M., Tsuchiya, H., Dick, L. F. P., & Schmuki, P. (2005). Initiation and Growth of Self-Organized TiO[sub 2] Nanotubes Anodically Formed in NH[sub 4]F∕(NH[sub 4])[sub 2]SO[sub 4] Electrolytes. Journal of The Electrochemical Society. https://doi.org/10.1149/1.2008980
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Contains information from the Semantic Scholar Academic Graph Datasets, made available under the ODC Attribution License (ODC-BY 1.0).
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