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In Situ Raman Spectroscopy of Anodic Films Formed on Copper and Silver in Sodium Hydroxide Solution
Abstract
In situ Raman spectroscopy and cyclic voltammetry have been used simultaneously to study anodic film growth and dissolution on Cu and Ag in strongly alkaline solution. On copper, Cu 2 O and another species, believed to be a hydroxide, were detected spectroscopically during anodic film formation. Raman spectra of electrochemically formed hydroxides on copper have not previously been reported. On silver, AgO was detected. Neither CuO nor Ag 2 O was observed by Raman spectroscopy, although for certain potentials, AgO was apparently produced by photochemical conversion of Ag 2 O . Experiments were performed using both the 488 nm line from an argon laser and the 647.1 nm line from a krypton laser. It was concluded that the detection of these thin film oxides was by spontaneous or resonant Raman scattering and did not involve surface enhanced Raman scattering (SERS).
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Cited by
Corrosion behavior of super-hydrophobic surface on copper in seawater
Liu, T., Chen, S., Cheng, S., Tian, J., Chang, X., & Yin, Y. (2007) · Electrochimica Acta · doi:10.1016/j.electacta.2007.06.072 · Cited by 323
Deng, Y., & Yeo, B. S. (2017) · ACS Catalysis · doi:10.1021/acscatal.7b02561 · Cited by 284
Zhao, H., Yue, Y., Fan, Y., Wang, J., Li, W., Wei, F., Liu, M., Yu, Y., Lu, W., & Zhang, G. (2022) · ChemSusChem · doi:10.1002/cssc.202201625 · Cited by 27
Metadata
- Authors
- Hamilton, J. C., Farmer, J. C., & Anderson, R. J.
- Venue
- Journal of The Electrochemical Society
- Publisher
- The Electrochemical Society
- Published
- 1986-04-01
- Volume
- 133
- Issue
- 4
- Pages
- 739-745
- ISSN
- 0013-4651 (ISSN-L)
- 1945-7111
- OpenAlex
- W2139371931
- Cited by
- 226
- References
- 0
- FWCI
- 2.25
- Type
- journal article
- Language
- en
- Open access
- closed
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- CoChat. (2026). Citation check: In Situ Raman Spectroscopy of Anodic Films Formed on Copper and Silver in Sodium Hydroxide Solution. https://app.cochat.ai/papers/10.1149/1.2108666
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- Hamilton, J. C., Farmer, J. C., & Anderson, R. J. (1986). In Situ Raman Spectroscopy of Anodic Films Formed on Copper and Silver in Sodium Hydroxide Solution. Journal of The Electrochemical Society. https://doi.org/10.1149/1.2108666
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