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Synthesis and Thermal Analyses of TiO2-Derived Nanotubes Prepared by the Hydrothermal Method
Abstract
TiO 2-derived nanotubes were prepared by hydrothermal treatment of TiO 2 powder in NaOH aqueous solution. High-temperature x-ray diffraction (HT-XRD) andthermogravimetry-differential thermal analysis (TG-DTA) demonstrated the formation of TiO 2 (B) phase (a metastable polymorph of titanium dioxide) from the nanotubes under heating at ∼800 °C, which indicates the as-prepared nanotubes should be composed of layered titanate, most probably as H 2 Ti 3 O 7·nH 2 O (n < 3). Dehydration behavior and phase transformation confirmed by the HT-XRD study have suggested reliable reaction path and have well-solved the contradictions on the nanotube-formation mechanism among previous studies.
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Cited by
One‐dimensional TiO2 Nanotube Photocatalysts for Solar Water Splitting
Ge, M., Li, Q., Cao, C., Huang, J., Li, S., Zhang, S., Chen, Z., Zhang, K., Al‐Deyab, S. S., & Lai, Y. (2017) · Advanced Science · doi:10.1002/advs.201600152 · Cited by 555
Vijayan, B., Dimitrijevic, N. M., Rajh, T., & Gray, K. (2010) · The Journal of Physical Chemistry C · doi:10.1021/jp104345h · Cited by 124
SYNTHESIS AND MICROSTRUCTURE OF A NOVEL TiO2 AEROGEL–TiO2 NANOWIRE COMPOSITE
SUZUKI, Y., BERGER, M.-H., D'ELIA, D., ILBIZIAN, P., BEAUGER, C., RIGACCI, A., HOCHEPIED, J.-F., & ACHARD, P. (2008) · Nano · doi:10.1142/s1793292008001222 · Cited by 6
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Metadata
- Authors
- Suzuki, Y., & Yoshikawa, S.
- Venue
- Journal of Materials Research
- Published
- 2004-04
- Volume
- 19
- Issue
- 4
- Pages
- 982-985
- ISSN
- 0884-1616 (ISSN-L)
- 0884-2914
- 2044-5326
- OpenAlex
- W2104564630
- Cited by
- 232
- References
- 0
- FWCI
- 12.52
- Type
- journal article
- Language
- en
- Open access
- closed
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