Analytical method validation of azadirachtin extracted from Azadirachta Indica
Open accessAbstract
A simple UV spectrophotometric method for the determination of Azadirachtin is developed exhibiting maximum absorbance using distilled water at 542nm.The present study is based on the detection of sample drug concentration using dichloro methane as diluent. All the conditions required were optimized. Statistical analysis was carried out and results of which were satisfactory. The optical characteristics such as absorption maxima, regression analysis and correlation coefficient are obtained. Recovery studies were close to 100% that indicate the accuracy and precision of proposed method and the non-interference of the formulation excipients. All the valid parameters are summarized.
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Azadirachtin was quantified using UV-VIS in accordance with the protocol published by Haq et al. (2017).
“The quantification of azadirachtin was performed using the UV-VIS technique in accordance with the protocol published by Haq et al. (2017), [29].”
From Optimized microwave-assisted azadirachtin extraction using response surface methodology (2024) · cites this paper as Haq et al. (2017), [29]
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Research works printed but not linked: 8
- AbdelouahebAlouani, NassimaRehimi, NoureddineSoltani (2009). Larvicidal activity of a neem tree extract (Azadirachtin) against mosquito larvae in the republic of Algeria. Jordon Journal of Biological Sciences. 2(1):15-22.
- Ambrosino, P., Fresa, R., Fogliano, V., Monti, S. M., &Ritieni, A. (1999). Extraction of azadirachtin A from neem seed kernels by supercritical fluid and its evaluation by HPLC and LC/MS. Journal of agricultural and food chemistry, 47(12), 5252-5256.
- Anas Rasheed, Dr. Osman Ahmed (2017). UPLC method optimization and validation for the estimation of sodium cromoglycate in pressurized metered dosage form. Int J App Pharm Sci Res. 2(2):18-24. http://dx.doi.org/10.21477/ijapsr.v2i2.7774. · DOI
- Anas Rasheed, Dr. Osman Ahmed (2017). Analytical development and validation of a stability-indicating method for the estimation of impurities in budesonide respules formulation. Int J App Pharm Sci Res. 2(3):46-54. http://dx.doi.org/10.21477/ijapsr.v2i3.8100 · DOI
- Anas Rasheed, Dr. Osman Ahmed (2017). Analytical separation and characterization of degradation products and the development and validation of a stability indicating method for the estimation of impurities in ipratropium bromide formulation. Int J App Pharm Sci Res. 2(3):55-63. http://dx.doi.org/10.21477/ijapsr.v2i3.8101 · DOI
- Anas Rasheed, Dr. Osman Ahmed (2017). Analytical separation and characterization of degradation products and the development and validation of a stability indicating method for the estimation of impurities in levosalbutamol respules formulation. Int J App Pharm Sci Res. 2(3):83-92. http://dx.doi.org/10.21477/ijapsr.v2i03.8254 · DOI
- Anas Rasheed, Dr. Osman Ahmed (2017). Analytical separation and characterization of degradation products and the development and validation of a stability indicating method for the estimation of impurities in montelukast oral dosage formulation. Int J App Pharm Sci Res. 2(3):69-77. http://dx.doi.org/10.21477/ijapsr.v2i03.8252. · DOI
- Anas Rasheed, Dr. Osman Ahmed (2017). UPLC method development and validation for the determination of chlophedianol hydrochloride in syrup dosage form. Int J App Pharm Sci Res. 2(2):18-24. http://dx.doi.org/10.21477/ijapsr.v2i2.7775. 31 · DOI
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Optimized microwave-assisted azadirachtin extraction using response surface methodology
Martínez-Castro, R., Flórez-Santiago, J., Valle-Molinares, R., Cabrera-Barraza, J., & Espitia-Almeida, F. (2024) · Heliyon · doi:10.1016/j.heliyon.2024.e31504 · Cited by 6 · see citing works
“The quantification of azadirachtin was performed using the UV-VIS technique in accordance with the protocol published by Haq et al. (2017), [29].”
Method
- Authors
- Ul Haq, S. I., Singh, T., Salman, S. M., Namreen, A., & Rasheed, A.
- Affiliations
- Guru Nanak Institutions (IN)
- Venue
- INTERNATIONAL JOURNAL OF APPLIED PHARMACEUTICAL SCIENCES AND RESEARCH
- Publisher
- Sierra Journals
- Published
- 2017-10-01
- Volume
- 2
- Issue
- 04
- Pages
- 99-106
- ISSN
- 2455-8095 (ISSN-L)
- OpenAlex
- W2757191448
- Cited by
- 7
- References
- 0
- Citations by year
- 2025: 1 · 2024: 2 · 2023: 1 · 2021: 2 · 2017: 1
- FWCI
- 0.19
- Type
- journal article
- Language
- en
- Open access
- diamond
- doi.org
- Licence
- Locations
- International Journal of Applied Pharmaceutical Sciences and Research (publishedVersion, cc-by-nc-nd)
- Sierra Journals - International Journal of Applied Pharmaceutical Sciences and Research (submittedVersion)
- Sierra Journals - International Journal of Applied Pharmaceutical Sciences and Research (submittedVersion, cc-by-nc-nd)
- Topics
- Physical Sciences › Chemistry › Analytical Chemistry › Analytical Methods in Pharmaceuticals
- Life Sciences › Agricultural and Biological Sciences › Plant Science › Insect Pest Control Strategies
- Life Sciences › Biochemistry, Genetics and Molecular Biology › Molecular Biology › Phytochemical compounds biological activities
- Keywords
- azadirachtin, Azadirachta indica, neem extract, UV spectrophotometric determination, analytical method validation, dichloromethane extraction, recovery and precision
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