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The Synthesis Process and Thermal Stability of V2C MXene
Open accessAbstract
The effect of etching solution on the synthesis process of two-dimensional vanadium carbide (V2C MXene) was researched. Three etching solutions were used to etch ternary carbide V2AlC at 90 °C. The three solutions were: lithium fluoride + hydrochloric acid (LiF + HCl), sodium fluoride + hydrochloric acid (LiF + HCl), and potassium fluoride + hydrochloric acid (KF + HCl). It was found that only NaF + HCl solution was effective for synthesizing highly pure V2C MXene. The existence of sodium (Na+) and chloridion (Cl−) in etching solution was essential for the synthesis. The thermal stability of the as-prepared V2C MXene in argon or air was studied. From thermogravimetry and differential thermal analysis, V2C MXene was found to be stable in argon atmosphere at a temperature of up to 375 °C. As the temperature increased, V2C MXene was gradually oxidized to form nanoparticles composed of vanadium trioxide (V2O3) and a part of V2C MXene was broken and transformed to vanadium carbide (V8C7) at 1000 °C. In air atmosphere, V2C MXene was stable at 150 °C. At 1000 °C, V2C MXene was oxidized to form vanadium pentoxide (V2O5).
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Cites
Two-Dimensional Molybdenum Carbide (MXene) as an Efficient Electrocatalyst for Hydrogen Evolution
Seh, Z. W., Fredrickson, K. D., Anasori, B., Kibsgaard, J., Strickler, A. L., Lukatskaya, M. R., Gogotsi, Y., Jaramillo, T. F., & Vojvodic, A. (2016) · ACS Energy Letters · doi:10.1021/acsenergylett.6b00247 · Cited by 1,482
Synthesis and thermal stability of two-dimensional carbide MXene Ti3C2
Li, Z., Wang, L., Sun, D., Zhang, Y., Liu, B., Hu, Q., & Zhou, A. (2015) · Materials Science and Engineering: B · doi:10.1016/j.mseb.2014.10.009 · Cited by 928 · cited 1×
“, studied the thermal stability of Ti3C2 in oxygen and argon [23].”
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Cited by
Emerging 2D MXenes for supercapacitors: status, challenges and prospects
Hu, M., Zhang, H., Hu, T., Fan, B., Wang, X., & Li, Z. (2020) · Chemical Society Reviews · doi:10.1039/d0cs00175a · Cited by 828
Metadata
- Authors
- Wu, M., Wang, B., Hu, Q., Wang, L., & Zhou, A.
- Venue
- Materials
- Publisher
- MDPI AG
- Published
- 2018-10-27
- Volume
- 11
- Issue
- 11
- Pages
- 2112
- ISSN
- 1996-1944 (ISSN-L)
- OpenAlex
- W2898602870
- Cited by
- 301
- References
- 2
- FWCI
- 5.60
- Type
- journal article
- Language
- en
- Open access
- gold
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Contains information from the Semantic Scholar Academic Graph Datasets, made available under the ODC Attribution License (ODC-BY 1.0).
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