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An Overview of Synthesis and Structural Regulation of Magnetic Nanomaterials Prepared by Chemical Coprecipitation

Li, Zelin, Sun, Yuanjun, Ge, Songwei, Zhu, Fei, Yin, Fei, Gu, Lina, Yang, Fan, Hu, Ping, Chen, Guoju, Wang, Kuaishe, Volinsky, Alex A.·2023·Metals
DOI 10.3390/met13010152
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Abstract

Magnetic nanomaterials are widely used in biosynthesis, catalysis, as electronic and microwave-absorbing materials, and in environmental treatment because of their high specific surface area, strong magnetism, chemical stability, and good biocompatibility. The chemical coprecipitation method is widely used for the preparation of magnetic nanomaterials due to its simplicity, low cost, and easily-controlled operating conditions. The magnetic nanomaterials prepared by the chemical coprecipitation method are summarized according to the different compositions, including the basic preparation principles, and the factors affecting their morphology, size, and microstructure. The mechanisms of preparing magnetic nanomaterials by chemical precipitation and the process control factors are emphasized. Finally, the preparation of magnetic nanomaterials by chemical coprecipitation is summarized and prospected.

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Figure 1 Flow chart of preparation of nanometer powder by chemical precipitation method. Figure 1. Flow chart of preparation of nanometer powder by chemical precipitation method.
Figure 1 Flow chart of preparation of nanometer powder by chemical precipitation method. Figure 1. Flow chart of preparation of nanometer powder by chemical precipitation method.CC-BY · From the PDF
Figure 2 ( a ) Variation of supersaturation of precipitation solution with time; ( b ) relationship between nucleation rate and supersaturation [18]. ( a , b ) Reprinted from Central South University, open access, Copyright (2022). Figure 2. ( a ) Variation of supersaturation of precipitation solution with time; ( b ) relationship between nucleation rate and supersaturation [18]. ( a , b ) Reprinted from Central South University, open access, Copyright (2022).
Figure 2 ( a ) Variation of supersaturation of precipitation solution with time; ( b ) relationship between nucleation rate and supersaturation [18]. ( a , b ) Reprinted from Central South University, open access, Copyright (2022). Figure 2. ( a ) Variation of supersaturation of precipitation solution with time; ( b ) relationship between nucleation rate and supersaturation [18]. ( a , b ) Reprinted from Central South University, open access, Copyright (2022).CC-BY · From the PDF
Figure 3 ( a ) Synthesis and ( b -d ) action diagrams of biomaterials [5,28-31]. ( a ) Reprinted from Chemical Engineering Journal C, 5416340606254, [30], Copyright (2022), with permission from Elsevier. ( b ) Reprinted from Materials Science & Engineering C, 5416251011560, [3], Copyright (2022), with permission from Elsevier. ( c ) Reprinted from International Journal of biomacromolecules, 1282828, [32], Copyright (2022), with permission from International Journal of biomacromolecules. ( d ) Reprinted from Colloids and Surfaces A: Physicochem. Eng. Aspects, 5416260383435, [26], Copyright (2022), with permission from Elsevier.
Figure 3 ( a ) Synthesis and ( b -d ) action diagrams of biomaterials [5,28-31]. ( a ) Reprinted from Chemical Engineering Journal C, 5416340606254, [30], Copyright (2022), with permission from Elsevier. ( b ) Reprinted from Materials Science & Engineering C, 5416251011560, [3], Copyright (2022), with permission from Elsevier. ( c ) Reprinted from International Journal of biomacromolecules, 1282828, [32], Copyright (2022), with permission from International Journal of biomacromolecules. ( d ) Reprinted from Colloids and Surfaces A: Physicochem. Eng. Aspects, 5416260383435, [26], Copyright (2022), with permission from Elsevier.CC-BY · From the PDF
Figure 4 ( a -c ) Catalyst mechanisms and functions, ( d ) structure diagram [49-61]. ( a ) Reprinted from Fuel, 5416481031506 [54], Copyright (2022), with permission from Elsevier. ( b ) Reprinted from Applied Surface Science, 54164800925859 [49], Copyright (2022), with permission from Elsevier. ( c ) Reprinted from Journal of Industrial and Engineering Chemistry, open access [44], Copyright (2022). ( d ) Reprinted from Journal of Zhejiang University-Science A, 5416481031506 [56], Copyright (2022), Figure 4. ( a -c ) Catalyst mechanisms and functions, ( d ) structure diagram [49-61]. ( a ) Reprinted from Fuel, 5416481031506 [54], Copyright (2022), with permission from Elsevier. ( b ) Reprinted from Applied Surface Science, 54164800925859 [49], Copyright (2022), with permission from Elsevier. ( c ) Reprinted from Journal of Industrial and Engineering Chemistry, open access [44], Copyright (2022). ( d ) Reprinted from Journal of Zhejiang University-Science A, 5416481031506 [56], Copyright (2022), with permission from Elsevier.
Figure 4 ( a -c ) Catalyst mechanisms and functions, ( d ) structure diagram [49-61]. ( a ) Reprinted from Fuel, 5416481031506 [54], Copyright (2022), with permission from Elsevier. ( b ) Reprinted from Applied Surface Science, 54164800925859 [49], Copyright (2022), with permission from Elsevier. ( c ) Reprinted from Journal of Industrial and Engineering Chemistry, open access [44], Copyright (2022). ( d ) Reprinted from Journal of Zhejiang University-Science A, 5416481031506 [56], Copyright (2022), Figure 4. ( a -c ) Catalyst mechanisms and functions, ( d ) structure diagram [49-61]. ( a ) Reprinted from Fuel, 5416481031506 [54], Copyright (2022), with permission from Elsevier. ( b ) Reprinted from Applied Surface Science, 54164800925859 [49], Copyright (2022), with permission from Elsevier. ( c ) Reprinted from Journal of Industrial and Engineering Chemistry, open access [44], Copyright (2022). ( d ) Reprinted from Journal of Zhejiang University-Science A, 5416481031506 [56], Copyright (2022), with permission from Elsevier.CC-BY · From the PDF
Figure 5 ( a -c ) Radar absorbing material performance characterization and radar absorbing mechanism [63,70]. ( a , c ) Reprinted from Journal of Materials Science, 5416520919952 [70], Copyright (2022), with permission from Elsevier. ( b ) Reprinted from Diamond and Related Materials, 5416520919952 [63], Copyright (2022), with permission from Elsevier.
Figure 5 ( a -c ) Radar absorbing material performance characterization and radar absorbing mechanism [63,70]. ( a , c ) Reprinted from Journal of Materials Science, 5416520919952 [70], Copyright (2022), with permission from Elsevier. ( b ) Reprinted from Diamond and Related Materials, 5416520919952 [63], Copyright (2022), with permission from Elsevier.CC-BY · From the PDF
Figure 6 The preparation process and mechanism of magnetic absorbing materials [82 Reprinted from Journal of Alloys and Compounds, 5416500493658 [78], Copyright (2022), mission from Elsevier. ( c ) Reprinted from Chemical Engineering Journal, 5416510964395 yright (2022), with permission from Elsevier. Figure 6. The preparation process and mechanism of magnetic absorbing materials [82,83]. ( a , b ) Reprinted from Journal of Alloys and Compounds, 5416500493658 [78], Copyright (2022), with permission from Elsevier. ( c ) Reprinted from Chemical Engineering Journal, 5416510964395 [77], Copyright (2022), with permission from Elsevier.
Figure 6 The preparation process and mechanism of magnetic absorbing materials [82 Reprinted from Journal of Alloys and Compounds, 5416500493658 [78], Copyright (2022), mission from Elsevier. ( c ) Reprinted from Chemical Engineering Journal, 5416510964395 yright (2022), with permission from Elsevier. Figure 6. The preparation process and mechanism of magnetic absorbing materials [82,83]. ( a , b ) Reprinted from Journal of Alloys and Compounds, 5416500493658 [78], Copyright (2022), with permission from Elsevier. ( c ) Reprinted from Chemical Engineering Journal, 5416510964395 [77], Copyright (2022), with permission from Elsevier.CC-BY · From the PDF
Figure 7 Steps of magnetic extraction in water environment [103]. Reprinted from Applied Science, open access, Copyright (2022). Figure 7. Steps of magnetic extraction in water environment [103]. Reprinted from Applied Science, open access, Copyright (2022).
Figure 7 Steps of magnetic extraction in water environment [103]. Reprinted from Applied Science, open access, Copyright (2022). Figure 7. Steps of magnetic extraction in water environment [103]. Reprinted from Applied Science, open access, Copyright (2022).CC-BY · From the PDF

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Metadata

Authors
Li, Z., Sun, Y., Ge, S., Zhu, F., Yin, F., Gu, L., Yang, F., Hu, P., Chen, G., Wang, K., & Volinsky, A. A.
Venue
Metals
Publisher
MDPI AG
Published
2023-01-11
Volume
13
Issue
1
Pages
152
ISSN
2075-4701
DOI
10.3390/met13010152
Cited by
60
References
0
Language
en
Licence
creativecommons.org/licenses/by/4.0/ (vor)
Funders
  • State Key Laboratory of Nickel and Cobalt Resources Comprehensive Utilization (GZSYS-KY-2020-017, 2022TD-30, 171101)
  • Scientific and Technological Innovation Team Project of Shaanxi Innovation Capability Support Plan, China (GZSYS-KY-2020-017, 2022TD-30, 171101)
  • Fok Ying Tung Education Foundation (GZSYS-KY-2020-017, 2022TD-30, 171101)
  • Youth Innovation Team of Shaanxi Universities (GZSYS-KY-2020-017, 2022TD-30, 171101)
  • Top young talents project of “Special support program for high-level talents” in the Shaanxi Province (GZSYS-KY-2020-017, 2022TD-30, 171101)

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Registry, retraction, Cites and statistics results are computed, not judged, with one exception: a printed reference that no index lists is read once by a model before it counts as a citation error. Claims are extracted by a model and kept only when their quote appears verbatim in the text; each cited source is then checked, with a model’s help, for whether it says what the claim relies on. Those verdicts can be wrong — read the claim’s quote and the cited source before relying on one.

Statistics and arithmetic are recomputed, not judged.

Confidence bands are shown only for fields calibrated on our annotated test set. None is calibrated yet, so no band is shown.

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