Cited by 931Mesoporous Materials and CatalysisSupercapacitor Materials and FabricationCarbon Dioxide Capture Technologies

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A Controllable Synthesis of Rich Nitrogen‐Doped Ordered Mesoporous Carbon for CO2 Capture and Supercapacitors

Wei, Jing, Zhou, Dandan, Sun, Zhenkun, Deng, Yonghui, Xia, Yongyao, Zhao, Dongyuan·2013·Advanced Functional Materials

DOI 10.1002/adfm.201202764

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Abstract

Abstract A controllable one‐pot method to synthesize N‐doped ordered mesoporous carbons (NMC) with a high N content by using dicyandiamide as a nitrogen source via an evaporation‐induced self‐assembly process is reported. In this synthesis, resol molecules can bridge the Pluronic F127 template and dicyandiamide via hydrogen bonding and electrostatic interactions. During thermosetting at 100 °C for formation of rigid phenolic resin and subsequent pyrolysis at 600 °C for carbonization, dicyandiamide provides closed N species while resol can form a stable framework, thus ensuring the successful synthesis of ordered N‐doped mesoporous carbon. The obtained N‐doped ordered mesoporous carbons possess tunable mesostructures (p6m and Im$ \bar 3 $ m symmetry) and pore size (3.1–17.6 nm), high surface area (494–586 m2 g−1), and high N content (up to 13.1 wt%). Ascribed to the unique feature of large surface area and high N contents, NMC materials show high CO2 capture of 2.8–3.2 mmol g−1 at 298 K and 1.0 bar, and exhibit good performance as the supercapacitor electrode with specific capacitances of 262 F g−1 (in 1 M H2SO4) and 227 F g−1 (in 6 M KOH) at a current density of 0.2 A g−1.

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Authors: Wei, J., Zhou, D., Sun, Z., Deng, Y., Xia, Y., & Zhao, D.
Affiliations: Fudan University (CN)
Corresponding author: Deng, Yonghui
Zhao, Dongyuan
ORCID: Wei, Jing
Zhou, Dandan
Sun, Zhenkun
Deng, Yonghui
Xia, Yongyao
Zhao, Dongyuan
Venue: Advanced Functional Materials
Publisher: Wiley
Published: 2012-12-07
Volume: 23
Issue: 18
Pages: 2322-2328
ISSN: 1616-301X (ISSN-L)
1616-3028
DOI: 10.1002/adfm.201202764
OpenAlex: W2058048032
Cited by: 931
References: 50
Citations by year: 2026: 12 · 2025: 25 · 2024: 34 · 2023: 38 · 2022: 49 · 2021: 71 · 2020: 72 · 2019: 91 · 2018: 107 · 2017: 115 · 2016: 122 · 2015: 95 · 2014: 75 · 2013: 24 · 2012: 1
FWCI: 28.64
Type: journal article
Language: en
Open access: closed
Licence: onlinelibrary.wiley.com/termsAndConditions#vor (vor)
Locations: Advanced Functional Materials (publishedVersion)
Topics: Physical Sciences › Materials Science › Materials Chemistry › Mesoporous Materials and Catalysis
Physical Sciences › Materials Science › Electronic, Optical and Magnetic Materials › Supercapacitor Materials and Fabrication
Physical Sciences › Chemical Engineering › Filtration and Separation › Carbon Dioxide Capture Technologies
Keywords: nitrogen-doped mesoporous carbon, ordered mesoporous carbon, dicyandiamide, nitrogen source, evaporation-induced self-assembly, resol phenolic resin, one-pot synthesis, CO2 capture, supercapacitor electrodes, specific capacitance, mesostructure control, pore size control

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A Controllable Synthesis of Rich Nitrogen‐Doped Ordered Mesoporous Carbon for CO2 Capture and Supercapacitors

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