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A Controllable Synthesis of Rich Nitrogen‐Doped Ordered Mesoporous Carbon for CO2 Capture and Supercapacitors
Abstract
Abstract A controllable one‐pot method to synthesize N‐doped ordered mesoporous carbons (NMC) with a high N content by using dicyandiamide as a nitrogen source via an evaporation‐induced self‐assembly process is reported. In this synthesis, resol molecules can bridge the Pluronic F127 template and dicyandiamide via hydrogen bonding and electrostatic interactions. During thermosetting at 100 °C for formation of rigid phenolic resin and subsequent pyrolysis at 600 °C for carbonization, dicyandiamide provides closed N species while resol can form a stable framework, thus ensuring the successful synthesis of ordered N‐doped mesoporous carbon. The obtained N‐doped ordered mesoporous carbons possess tunable mesostructures (p6m and Im$ \bar 3 $ m symmetry) and pore size (3.1–17.6 nm), high surface area (494–586 m2 g−1), and high N content (up to 13.1 wt%). Ascribed to the unique feature of large surface area and high N contents, NMC materials show high CO2 capture of 2.8–3.2 mmol g−1 at 298 K and 1.0 bar, and exhibit good performance as the supercapacitor electrode with specific capacitances of 262 F g−1 (in 1 M H2SO4) and 227 F g−1 (in 6 M KOH) at a current density of 0.2 A g−1.
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“A large variety of mesoporous metal oxides in the form of powder were synthesized through EISA using commercial Pluronics as a template [149].”
From Block Copolymers: Synthesis, Self-Assembly, and Applications (2017) · cites this paper as [149]
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Self-citation
Metadata
- Authors
- Wei, J., Zhou, D., Sun, Z., Deng, Y., Xia, Y., & Zhao, D.
- Affiliations
- Fudan University (CN)
- Corresponding author
- Deng, Yonghui
- Zhao, Dongyuan
- Venue
- Advanced Functional Materials
- Publisher
- Wiley
- Published
- 2012-12-07
- Volume
- 23
- Issue
- 18
- Pages
- 2322-2328
- ISSN
- 1616-301X (ISSN-L)
- 1616-3028
- OpenAlex
- W2058048032
- Cited by
- 931
- References
- 50
- Citations by year
- 2026: 12 · 2025: 25 · 2024: 34 · 2023: 38 · 2022: 49 · 2021: 71 · 2020: 72 · 2019: 91 · 2018: 107 · 2017: 115 · 2016: 122 · 2015: 95 · 2014: 75 · 2013: 24 · 2012: 1
- FWCI
- 28.64
- Type
- journal article
- Language
- en
- Open access
- closed
- Locations
- Advanced Functional Materials (publishedVersion)
- Topics
- Physical Sciences › Materials Science › Materials Chemistry › Mesoporous Materials and Catalysis
- Physical Sciences › Materials Science › Electronic, Optical and Magnetic Materials › Supercapacitor Materials and Fabrication
- Physical Sciences › Chemical Engineering › Filtration and Separation › Carbon Dioxide Capture Technologies
- Keywords
- nitrogen-doped mesoporous carbon, ordered mesoporous carbon, dicyandiamide, nitrogen source, evaporation-induced self-assembly, resol phenolic resin, one-pot synthesis, CO2 capture, supercapacitor electrodes, specific capacitance, mesostructure control, pore size control
About these checks
Registry, retraction, Cites and statistics results are computed, not judged, with one exception: a printed reference that no index lists is read once by a model before it counts as a citation error. Claims are extracted by a model and kept only when their quote appears verbatim in the text; each cited source is then checked, with a model’s help, for whether it says what the claim relies on. Those verdicts can be wrong — read the claim’s quote and the cited source before relying on one.
Statistics and arithmetic are recomputed, not judged.
Confidence bands are shown only for fields calibrated on our annotated test set. None is calibrated yet, so no band is shown.
What counts as a claim ›How we measure confidence ›How we check this ›
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