Cited by 276Advanced Photocatalysis Techniques2D Materials and ApplicationsTiO2 Photocatalysis and Solar Cells

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Drastic Layer‐Number‐Dependent Activity Enhancement in Photocatalytic H2 Evolution over n MoS2/CdS (n ≥ 1) Under Visible Light

Chang, Kun, Li, Mu, Wang, Tao, Ouyang, Shuxin, Li, Peng, Liu, Lequan, Ye, Jinhua·2015·Advanced Energy Materials

DOI 10.1002/aenm.201402279

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Abstract

Exploiting noble‐metal‐free cocatalysts is of huge interest for photocatalytic water splitting using solar energy. As an efficient cocatalyst in photocatalysis, MoS 2 is shown promise as a low‐cost alternative to Pt for hydrogen evolution. Here we report a systematical study on controlled synthesis of MoS 2 with layer number ranging from ≈1 to 112 and their activities for photocatalytic H 2 evolution over commercial CdS. A drastic increase in photocatalytic H 2 evolution is observed with decreasing MoS 2 layer number. Particularly for the single‐layer (SL) MoS 2, the SL‐MoS 2/CdS sample reaches a high H 2 generation rate of ≈2.01 × 10−3m h−1 in Na 2 S–Na 2 SO 3 solutions and ≈2.59 × 10−3m h−1 in lactic acid solutions, corresponding to an apparent quantum efficiency of 30.2% and 38.4% at 420 nm, respectively. In addition to the more exposed edges and unsaturated active S atoms, valence band–XPS and Mott–Schottky plots analysis indicate that the SL MoS 2 has the more negative conduction band energy level than the H+/H 2 potential, facilitating the hydrogen reduction.

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Authors: Chang, K., Li, M., Wang, T., Ouyang, S., Li, P., Liu, L., & Ye, J.
Affiliations: National Institute for Materials Science (JP)
Tianjin University (CN)
Corresponding author: Ye, Jinhua
ORCID: Chang, Kun
Li, Mu
Wang, Tao
Ouyang, Shuxin
Li, Peng
Liu, Lequan
Ye, Jinhua
Venue: Advanced Energy Materials
Publisher: Wiley
Published: 2015-03-12
Volume: 5
Issue: 10
ISSN: 1614-6832 (ISSN-L)
1614-6840
DOI: 10.1002/aenm.201402279
OpenAlex: W2026392595
Cited by: 276
References: 55
Citations by year: 2026: 3 · 2025: 12 · 2024: 19 · 2023: 21 · 2022: 24 · 2021: 20 · 2020: 37 · 2019: 35 · 2018: 34 · 2017: 37 · 2016: 26 · 2015: 8
FWCI: 10.36
Type: journal article
Language: en
Open access: closed
Licence: onlinelibrary.wiley.com/termsAndConditions#vor (vor)
Locations: Advanced Energy Materials (publishedVersion)
Topics: Physical Sciences › Energy › Renewable Energy, Sustainability and the Environment › Advanced Photocatalysis Techniques
Physical Sciences › Materials Science › Materials Chemistry › 2D Materials and Applications
Physical Sciences › Energy › Renewable Energy, Sustainability and the Environment › TiO2 Photocatalysis and Solar Cells
Keywords: photocatalytic hydrogen evolution, MoS2, CdS, layer number dependence, monolayer MoS2, visible light photocatalysis, noble-metal-free cocatalyst, photocatalytic water splitting, conduction band energy level, apparent quantum efficiency

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Drastic Layer‐Number‐Dependent Activity Enhancement in Photocatalytic H2 Evolution over n MoS2/CdS (n ≥ 1) Under Visible Light

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