Cited by 1,428Electrocatalysts for Energy ConversionCO2 Reduction Techniques and CatalystsIron oxide chemistry and applications

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Ultrathin Spinel‐Structured Nanosheets Rich in Oxygen Deficiencies for Enhanced Electrocatalytic Water Oxidation

Bao, Jian, Zhang, Xiaodong, Fan, Bo, Zhang, Jiajia, Zhou, Min, Yang, Wenlong, Hu, Xin, Wang, Hui, Pan, Bicai, Xie, Yi·2015·Angewandte Chemie International Edition

DOI 10.1002/anie.201502226

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Abstract

Electrochemical water splitting is a clean technology for H2 fuels, but greatly hindered by the slow kinetics of the oxygen evolution reaction (OER). Herein, a series of spinel-structured nanosheets with oxygen deficiencies and ultrathin thicknesses were designed to increase the reactivity and the number of active sites of the catalysts, which were then taken as an excellent platform for promoting the water oxidation process. Theoretical investigations showed that the oxygen vacancies confined in the ultrathin nanosheet could lower the adsorption energy of H2O, leading to increased OER efficiency. As expected, the NiCo2O4 ultrathin nanosheets rich in oxygen vacancies exhibited a large current density of 285 mA cm(-2) at 0.8 V and a small overpotential of 0.32 V, both of which are superior to the corresponding values of bulk samples or samples with few oxygen deficiencies and even higher than those of most reported non-precious-metal catalysts. This work should provide a new pathway for the design of advanced OER catalysts.

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Authors: Bao, J., Zhang, X., Fan, B., Zhang, J., Zhou, M., Yang, W., Hu, X., Wang, H., Pan, B., & Xie, Y.
Affiliations: University of Science and Technology of China (CN)
Technische Universität Ilmenau (DE)
Corresponding author: Zhang, Xiaodong
Xie, Yi
ORCID: Bao, Jian
Zhang, Xiaodong
Zhang, Jiajia
Zhou, Min
Yang, Wenlong
Hu, Xin
Pan, Bicai
Xie, Yi
Venue: Angewandte Chemie International Edition
Publisher: Wiley
Published: 2015-05-07
Volume: 54
Issue: 25
Pages: 7399-7404
ISSN: 1433-7851 (ISSN-L)
1521-3773
DOI: 10.1002/anie.201502226
OpenAlex: W2151061566
Cited by: 1,428
References: 34
Citations by year: 2026: 55 · 2025: 90 · 2024: 123 · 2023: 120 · 2022: 153 · 2021: 174 · 2020: 196 · 2019: 187 · 2018: 156 · 2017: 105 · 2016: 55 · 2015: 14
FWCI: 32.52
Type: journal article
Language: en
Open access: closed
Licence: onlinelibrary.wiley.com/termsAndConditions#vor (vor)
Locations: Angewandte Chemie International Edition (publishedVersion)
PubMed (publishedVersion)
Topics: Physical Sciences › Energy › Renewable Energy, Sustainability and the Environment › Electrocatalysts for Energy Conversion
Physical Sciences › Energy › Renewable Energy, Sustainability and the Environment › CO2 Reduction Techniques and Catalysts
Physical Sciences › Materials Science › Materials Chemistry › Iron oxide chemistry and applications
Keywords: oxygen evolution reaction, electrocatalytic water oxidation, oxygen vacancies, ultrathin nanosheets, NiCo2O4, non-noble metal catalysts, water splitting, hydrogen production, water adsorption energy

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Ultrathin Spinel‐Structured Nanosheets Rich in Oxygen Deficiencies for Enhanced Electrocatalytic Water Oxidation

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