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Definitive Molecular Level Characterization of Defects in UiO‐66 Crystals
Abstract
The identification and characterization of defects, on the molecular level, in metal‐organic frameworks (MOFs) remain a challenge. With the extensive use of single‐crystal X‐ray diffraction (SXRD), the missing linker defects in the zirconium‐based MOF UiO‐66, Zr 6 O 4(OH)4(C 8 H 4 O 4)6, have been identified as water molecules coordinated directly to the zirconium centers. Charge balancing is achieved by hydroxide anions, which are hydrogen bonded within the pores of the framework. Furthermore, the precise nature of the defects and their concentration can be manipulated by altering the starting materials, synthesis conditions, and post‐synthetic modifications.
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The nature of the active site in heterogeneous metal catalysis
Nørskov, J. K., Bligaard, T., Hvolbæk, B., Abild-Pedersen, F., Chorkendorff, I., & Christensen, C. H. (2008) · Chemical Society Reviews · doi:10.1039/b800260f · Cited by 885
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Metal–organic frameworks for membrane-based separations
Denny, M. S., Moreton, J. C., Benz, L., & Cohen, S. M. (2016) · Nature Reviews Materials · doi:10.1038/natrevmats.2016.78 · Cited by 820
Winarta, J., Shan, B., Mcintyre, S. M., Ye, L., Wang, C., Liu, J., & Mu, B. (2020) · Crystal Growth & Design · doi:10.1021/acs.cgd.9b00955 · Cited by 641
Imaging defects and their evolution in a metal–organic framework at sub-unit-cell resolution
Liu, L., Chen, Z., Wang, J., Zhang, D., Zhu, Y., Ling, S., Huang, K.-W., Belmabkhout, Y., Adil, K., Zhang, Y., et al. (2019) · Nature Chemistry · doi:10.1038/s41557-019-0263-4 · Cited by 579
Stable Metal–Organic Frameworks with Group 4 Metals: Current Status and Trends
Yuan, S., Qin, J.-S., Lollar, C. T., & Zhou, H.-C. (2018) · ACS Central Science · doi:10.1021/acscentsci.8b00073 · Cited by 561
Covalent Chemistry beyond Molecules
Jiang, J., Zhao, Y., & Yaghi, O. M. (2016) · Journal of the American Chemical Society · doi:10.1021/jacs.5b10666 · Cited by 448
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Metadata
- Authors
- Trickett, C. A., Gagnon, K. J., Lee, S., Gándara, F., Bürgi, H., & Yaghi, O. M.
- Venue
- Angewandte Chemie International Edition
- Publisher
- Wiley
- Published
- 2015-08-07
- Volume
- 54
- Issue
- 38
- Pages
- 11162-11167
- ISSN
- 1433-7851 (ISSN-L)
- 1521-3773
- OpenAlex
- W2113510568
- Cited by
- 526
- References
- 1
- FWCI
- 16.35
- Type
- journal article
- Language
- en
- Open access
- closed
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- Trickett, C. A., Gagnon, K. J., Lee, S., Gándara, F., Bürgi, H., & Yaghi, O. M. (2015). Definitive Molecular Level Characterization of Defects in UiO‐66 Crystals. Angewandte Chemie International Edition. https://doi.org/10.1002/anie.201505461
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